NYC 9/11 Public Portal Document
121 RcvAcwEt)
Data File : C:\MSDCHEM\1\DATA\053002\LBB0530.D Vial: 15
Acq On : 30 May 2002 12:04 pm Operator: Bohlk / Inst 213
Sample : LB 5/23/02 Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: rteint.p
Quant Time: Jun 03 16:10:19 2002 Quant Results File: 052802.RES
Quant Method : C:\MSDCHEM\l\5973N\052802.M (RTE Integrator) 27
Title : Quantitation For Method 525.2 ores
Last Update : Mon Jun 03 15:34:22 2002
Response via : Initial Calibration
DataAcq Meth : 052802
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-dlO 18.19 164 2156780 5.00 ug/L 0.00
9) Phenanthrene d-10 22.51 188 3205430 5.00 ug/L 0.00
19) Chrysene d-12 30.29 240 2157119 5.00 ug/L 0.00
25) p-Terphenyl d-14 27.39 244 2442452 5.00 ug/L 0.00
System Monitoring Compounds
2) 1,3-Dimethyl-2-nitrobenzen 13.11 134 588437 4.86 ug/L 0.00
Spiked Amount 5.000 Recovery = 97.20%
20) Triphenyl Phosphate 29.57 326 482325 5.26 ug/L 0.00
Spiked Amount 5.000 Recovery = 105.20%
21) Perylene D-12 34.30 264 1127302 3.92 ug/L 0.00
Spiked Amount 5.000 Recovery = 78.40%
26) Acenaphthene d-10 (surr) 18.19 164 2156780 3.97 ug/L 0.00
Spiked Amount 5.000 Recovery = 79.40%
27) Phenanthrene d-10 (surr) 22.51 188 3205430 . 4.23 ug/L 0.00
Spiked Amount 5.000 Recovery = 84.60%
2 8) Chrysene d-12 (surr) 30.29 240 2157119 4.34 ug/L 0.00
Spiked Amount 5.000 Recovery = 86.80%
Target Compounds Qvalue
3) Hexachlorocyclopentadiene 0.00 237 0 N.D.
4) Hexachlorobenzene 0.00 284 0 N.D.
5) EPTC 0.00 128 0 N.D.
6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
7) 2,4-Dinitotoluene 0.00 165 0 N.D.
8) Molinate 0.00 126 0 N.D.
10) Simazine 0.00 201 0 N.D.
11) Atrazine 0.00 200 0 N.D.
12) Alachlor 0.00 160 0 N.D.
13) Terbacil 0.00 117 0 N.D.
14) Acetochlor 0.00 146 0 N.D.
15) Metribuzin 0.00 198 0 N.D.
16) Metolachlor 0.00 162 0 N.D.
17) Butachlor 0.00 160 0 N.D. d
18) 4,4'-DDE 0.00 246 0 N.D. d
22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. d
23) Bis (2-Ethylhexyl) phthala 30.95 149 114289 0.92 ug/L 96
24) Benzo (a) pyrene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBB0530.D 052802.M Mon Jun 03 16:11:13 2002 Page 1
NYC-WTC_000012583
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