NYC 9/11 Public Portal Document
Quantitation Report (Not Reviewed)
Data File : C:\MSDCHEM\1\DATA\053002\C1B0530.D Vial: 6
• Acq On : 30 May 2002 10:33 am Operator: Bohlk / Inst 213
Sample : CAL 1.0 UG/L Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: rteint.p
Quant Time: Jun 03 16:08:35 2002 Quant Results File: 052802.RES
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Quant Method : C:\MSDCHEM\l\5973N\052802.M (RTE Integrator)
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Title : Quantitation For Method 525.2
Last Update : Mon Jun 03 15:34:22 2002
Response via : Initial Calibration
DataAcq Meth : 052802
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-dlO 18.19 164 2289508 5.00 ug/L 0.00
9) Phenanthrene d-10 22.51 188 3268580 5.00 ug/L 0.00
19) Chrysene d-12 30.29 240 2113822 5.00 ug/L 0.00
25) p-Terphenyl d-14 27.39 244 1852377 5.00 ug/L 0.00
System Monitoring Compounds
2) 1,3 -Dimethyl -2 -nitrobenzen 13.11 134 649043 5.05 ug/L 0.00
Spiked Amount 5.000 Recovery = 101.00%
20) Triphenyl Phosphate 29.57 326 461491 5.14 ug/L 0.00
Spiked Amount 5.000 Recovery = 102.80%
21) Perylene D-12 34.30 264 1351725 4.80 ug/L 0.00
Spiked Amount 5.000 Recovery = 96.00%
26). Acenaphthene d-10 (surr) 18.19 164 2289508 5.56 ug/L 0.00
Spiked Amount 5.000 Recovery = 111.20%
27) Phenanthrene d-10 (surr) 22.51 188 3268580 \ 5.68 ug/L 0.00
Spiked Amount 5.000 Recovery = 113.60%
28) Chrysene d-12 (surr) 30.29 240 2113822 5.61 ug/L 0.00
Spiked Amount 5.000 Recovery = 112.20%
Target Compounds Qvalue
3) Hexachlorocyclopentadiene 15.68 237 53725 1.63 ug/L 98
4) Hexachlorobenzene 21.37 284 132634 1.02 ug/L 93
5) EPTC 16.16 128 204056 0.99 ug/L 98
6) 2,6-Dinitrotoluene 17.75 165 65682 1.35 ug/L 97
7) 2,4-Dinitotoluene 18.89 165 74568 1.43 ug/L 98
8) Molinate 19.08 126 299626 1.02 ug/L 99
10) Simazine 21.90 201 66796 1.09 ug/L 93
11) Atrazine 22.02 200 112705 0.90 ug/L 91
12) Alachlor 23.89 160 113568 0.91 ug/L # 37
13) Terbacil 22.81 117 38727 1.67 ug/L 92
14) Acetochlor 23.67 146 69686 0.74 ug/L 85
15) Metribuzin 23.71 198 95735 1.19 ug/L 98
16) Metolachlor 24.82 162 311048 0.99 ug/L 97
17) Butachlor 26.64 160 91942 1.05 ug/L 92
18) 4,4’-DDE 27.28 246 110483 0.97 ug/L 96
22) Bis (2-Ethylhexyl) adipate 29.51 129 144932 1.39 ug/L 99
23) Bis (2-Ethylhexyl) phthala 30.95 149 246344 1.19 ug/L 98
24) Benzo (a) pyrene 34.15 252 222640 0.97 ug/L 99
(#) = qualifier out of range (m) = manual integration
C1B0530.D 052802.M Mon Jun 03 16:08:58 2002 Page 1
NYC-WTC_000012563
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