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← Document results/DEP Box 15/525 NOT OVR SAMPLE
Document / 5 pages

GCMS pesticide analysis results, sample AE11911, May-June 2002

Machine-extracted title · confidence 100%

Laboratory report listing analytical results for pesticides and related compounds in a reference standard sample.

NYC-WTC_000012610–000012614

Folder label: “525 NOT OVR SAMPLE

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NYC 9/11 Public Portal Document yUaitLtce.ii CCPUL t 191 RCVLSwct)

Data" File : C:\MSDCHEM\1\DATA\053002\11911B.D Vial: 26 Acq On : 30 May 2002 12:49 pm Operator: Bohlk / Inst 213 ' Sample : SAMPLE 11911 REINJD Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jun 03 16:12:31 2002 Quant Results File: 052802.RES

Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 *‘* Last Update : Mon Jun 03 15:34:22 2002 Response via : Initial Calibration DataAcq Meth : 052802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.19 164 2672647 5.00 ug/L 0.00 9) Phenanthrene d-10 22.51 188 3975265 5.00 ug/L 0.00 19) Chrysene d-12 30.30 240 2574533 5.00 ug/L 0.00 25) p-Terphenyl d-14 27.39 244 2943363 5.00 ug/L 0.00

System Monitoring Compounds 2) l,3-Dimethyl-2-nitrobenzen 13.11 134 728943 4.86 ug/L 0.00 Spiked Amount 5.000 Recovery = 97.20% 20) Triphenyl Phosphate 29.57 326 611069 5.58 ug/L 0.00 Spiked Amount 5.000 Recovery = 111.60% 21) Perylene D-12 34.30 264 1638847 4.78 ug/L 0.00 Spiked Amount 5.000 Recovery = 95.60% 26) Acenaphthene d-10 (surr) 18.19 164 2672647 4.09 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.80% 27) Phenanthrene d-10 (surr) 22.51 188 3975265 v 4.35 ug/L 0.00 Spiked Amount 5.000 Recovery = 87.00% 28) Chrysene d-12 (surr) 30.30 240 2574533 4.30 ug/L 0.00 Spiked Amount 5.000 Recovery = 86.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. d 23) Bis (2-Ethylhexyl) phthala 30.95 149 266387 1.14 ug/L 95 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 11911B.D 052802.M Mon Jun 03 16:13:11 2002 Page 1

NYC-WTC_000012613

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NYC-WTC_000012613Source: NYC Law Department, mirrored locally

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