Quality control spiked sample analysis for pesticide testing method 525.2, completed June 28, 2002, with recovery percentages for known pesticide analytes.
NYC-WTC_000012585–000012587Folder label: “525 NOT OVR SAMPLE”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document gudt. uauj.ua RCpOA L (21 REVLSwwUJ
Data File : C:\MSDCHEM\1\DATA\052902\11555.D Vial: 21 Acq On : 29 May 2002 6:31 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11555 5/23/02 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: rteint.p Quant Time: Jun 03 15:56:40 2002 Quant Results File: 052802.RES
Quant Method : C:\MSDCHEM\l\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon Jun 03 15:34:22 2002 Response via : initial Calibration DataAcq Meth : 052802
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 18.19 164 2016122 5.00 ug/L 0.00 9) Phenanthrene d-10 22.51 188 2838112 5.00 ug/L 0.00 19) Chrysene d-12 30.29 240 1880511 5.00 ug/L 0.00 25) p-Terphenyl d-14 27.39 244 2281168 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3 -Dimethyl -2 -nitrobenzen 13.11 134 564136 4.99 ug/L 0.00 Spiked Amount 5.000 Recovery - 99.80% 20) Triphenyl Phosphate 29.57 326 476714 5.96 ug/L 0.00 Spiked Amount 5.000 Recovery = 119.20% 21) Perylene D-12 34.30 264 1251428 4.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.80% 26) Acenaphthene d-10 (surr) 18.19 164 2016122 3.98 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.60% 27) Phenanthrene d-10 (surr) 22.51 188 2838112 4.01 ug/L 0.00 Spiked Amount 5.000 Recovery = 80.20% 28) Chrysene d-12 (surr) 30.29 240 1880511 4.05 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.00%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. d 23) Bis (2-Ethylhexyl) phthala 30.95 149 154862 1.05 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration 11555.D 052802.M Mon Jun 03 15:57:14 2002 Page 1
NYC-WTC_000012586
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NYC-WTC_000012610
Laboratory report listing analytical results for pesticides and related compounds in a reference standard sample.
1 shared topics · Same agency, volume and box · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012597
Laboratory report providing analytical data for pesticides and related compounds in a duplicate spiked water sample.
1 shared topics · Same agency, volume and box · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015978
Laboratory report showing quality control checks for pesticides and organic compounds in sample AE11755 analyzed on May 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.980
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016014
Laboratory report listing pesticide and organic compound concentrations in sample AE11755 analyzed between May 10 and May 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.980
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015989
Laboratory report showing field blank test results for pesticide and organic compounds in sample AE10997 analyzed on May 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.977
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012554
Laboratory report for sample AE11555 listing detection results for DDT and other pesticides in micrograms per unit.
1 shared topics · Same agency, volume and box · similarity 0.977
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012593
Laboratory report detailing analytical results for pesticides and related compounds in a spiked water sample.
1 shared topics · Same agency, volume and box · similarity 0.976
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012588
Quality control spiked sample analysis for pesticide testing method 525.2, completed June 28, 2002, with recovery percentages for known pesticide analytes.
Same agency, volume and box · similarity 0.972
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015981
Laboratory report listing pesticide and organic compound concentrations in sample AE10996 analyzed between May 10 and May 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.968
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015985
Laboratory report listing pesticide and organic compound concentrations in sample AE10997 analyzed between May 10 and May 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.968
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000082542
Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.
1 shared topics · similarity 0.976
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000082503
Results for calibration standards including hexachlorobenzene and simazine from sample AE10186 analyzed on May 2, 2002.
1 shared topics · similarity 0.970
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000012503
Department of Environmental Protection record regarding sample collection or analysis at the 525 site.
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NYC-WTC_000012504
Laboratory worksheet recording extraction parameters and analytical conditions for GCMS sample processing.
Filed in the same folder
NYC-WTC_000012511
Chromatographic data file from May 28, 2002 showing instrument analysis of DFTPP and Endrin standards.
Filed in the same folder
NYC-WTC_000012543
Laboratory report for sample AE11555 listing detection results for DDT and other pesticides in micrograms per unit.
Filed in the same folder
NYC-WTC_000012554
Laboratory report for sample AE11555 listing detection results for DDT and other pesticides in micrograms per unit.
Filed in the same folder