GCMS Analysis Report, Sample AE04247, Apr 2002

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Data File : C:\MSDCHEM\1\DATA\032602\4247.D Vial: 4 Acq On : 26 Mar 2002 1:19 pm Operator: McLean Sample : 2/28/02 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Phenanthrene-diO Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.23 ug/L 96610 Phenanthrene -dl0 22.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-diO 188 C14D10 001517-22-2 59 2 Acridine-D9 188 C13D9N 000000-00-0 50 3 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 000000-00-0 50 4 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 50 Abundance Scan 3330 (22.645 min): 4247.D (-) m/z 188.20 100.00% 188

5000

160 ....rr l | r l . r. rr I I | 1 1 l' 80 95 22.40 22.60 22,80 23.00 42 52 64 |_____________ 146 . III m/z 160.15 22.59% 01 51** ' t ■ ■ ■ ■ i ■ ■ ■ ' i ‘ 1 1 m/z-> 20 40 60 80 100 120 140 160 180 Abundance #84499: Phenanthrene-d10 188

5000 Tpe TTTr IrT 22.40 22.60 22.80 23.00 m/z 94.80 14.84% 80 94 160 30 42 52 66 „|| ..108118 132 146 il 170 Of - 1’1 I'l l I I | 1* 1""" ■ I'l ITT rn/z-> 20 40 60 80 100 120 140 160 ■180 Abundance #85255: Acridine-D9 188

-n-p-r ' ‘ I ‘ ‘ 1 ' I ‘ ■ 22.40 22.60 22.80 23.00 5000 m/z 80.10 14.40%

93 158 66 80 . 0t .16.28. 42 52 TIT11-THTPr 106118 ! 132 146, # CT , 4 m/z-> 20 40 60I 80 100 120 140 160 180 Abundance #98580: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 188 22.40 22.60 22.80 23.00 m/z 185.10 13.56%

5000 79 91

55 67 105 131 145 159 7 117 m/z—> 0 । । |-1 i i r| > 1 r’" । i h 20 40 60 I80 ---4A+173, 100 120 140 160 180 ■, , ! pr 22.40 22.60 22.80 23.00

4247.D 032802.M Mon Apr 01 08:06:35 2002 Page 3

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