NYC-WTC_000058391
Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04592.
1 shared topics · similarity 0.998
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GCMS analysis results for sample AE04411, April 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of environmental sample AE04411 conducted on April 3, 2002.
NYC-WTC_000011877–000011892Folder label: “GCMS X 2/28/02 A 3/26/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\MAR2502\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
14.85 0.53 ug/1 89404 Naphthalene-d8 15.89
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 N- (Trifluoroacetyl) -N,O,O' ,0’ '-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 Silane, [ [4- [1,2-bis [ (trimethylsily 458 C20H42O4Si4 056114-62-6 43 4 Benzoic ” hudonpo acid, ′ 2,Cron 4-bis [ (trimethylsil 370 C16H3004Si3 1naa ha *51 minAmin 4 — 73 010586-16-0 00 100 00% 38 Abundance Scan 1068 (14.851 min): 4411.D (-) 73
267 355 5000- ....... H 45 14.60 14.80 15.00 15.20 323 —1 103 154.193. 237. 1 . 1 ‘ i ‘ ‘ ' i 1 ■ ■ ■ I ' 1 m/z 267.00 52.86% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 14.60 14.80 15.00 15.20 m/z 355.05 51.65% 207 , 'rl 1 ' ‘ ‘ I ‘ ‘ ‘ ‘ 1 ‘ ‘ ‘ ' I • ' ‘ ‘ i ‘ ‘ 1 ‘ I ‘ 323.1 : ■ ■ i ■ ■ ■ ■ i ‘ • 1 i ■ ■ ■ ' 1 1 1 50 100 150 200 250 3001 350 400 450 500 550 Abundance #8C10, 01-4.0,0 ) • tii ana 1. 73 ....... L,....... 16**I***‘I‘11**1* 355 14.60 14.80 15.00 15.20 5000 m/z 356.0,5 A 17.84%
45 147 193 267 538 m/z-> Abundance 50 100 150 200 250 300 350 400 #74512: Silane. [[4-[1,2-bis[(trimethylsilyl)oxylethy]-1,2 3$5 450 500 550 ...... H..... . 14.60 14.80 15.00 15.20 m/z 268.00 13.97% 73 5000
147 I 179 207 251 281 443 1 • I t ■ ■ ■ i ■ ‘ ■ I ■ ' 1 TTn1*-n——TIC———"1‘ 1 ‘ i 1 ' i ■ ‘ m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20
4411.D GCMS0308.M Thu Mar 28 12:33:40 2002 Page 1
NYC-WTC_000011884
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NYC-WTC_000011884Source: NYC Law Department, mirrored locally
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