GCMS calibration table for TCLP method, March 2002

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Instrument output displaying calibration data and surrogate recovery results for sample AE03265.

NYC-WTC_000011407–000011414

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02”

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\3265.D Vial: 40 Acq On 3 Mar 2002 2:39 am Operator: - Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 6 11:25 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.32 152 695192 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 2713675 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.28 164 1422526 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.73 188 2105739 20.00 ug/1 -0.04 38) Chrysene-dl2 33.79 240 1412320 20.00 ug/1 -0.06 44) Perylene-dl2 38.08 264 938913 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD 30.80 235 57565 2.62 ug/mL 0.30 Spiked Amount 5.000 Recovery = 52.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.02 128 453 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.63 163 1175 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 20.80 152 184 N.D. 2 3) Acenaphthene 21.36 153 214 N.D. 24) 2,4-Dinitrotoluene 21.69 165 442 N.D. 25) Diethylphthalate 22.76 149 1522 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

•(#) = qualifier out of range (m) = manual integration 3265.D GCMS0208.M Mon Mar 25 12:02:05 2002 Page 1

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GCMS calibration table for TCLP method, March 2002 · Box DEP Box 14

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Instrument output displaying calibration data and surrogate recovery results for sample AE03283.

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