GCMS analysis results for sample AE02721, March 5 2002

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Library Search Compound Report ’* Data File : C: \MSDCHEM\1\5973N\02FEB28\02721.D Vial: 6 Acq On : 28 Feb 2002 6:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 METHYL-2-DEOXY-L-FUCOSIDE Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

13.39 0.07 ug/L 38017 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 METHYL-2-DEOXY-L-FUCOSIDE 162 C7H14O4 000000-00-0 9 2 2-Cyclopenten-l-one, 3-(acetyloxy)- 140 C7H803 018766-96-6 5 3 Methenamine 140 C6H12N4 000100-97-0 4 4 2-Hydroxy-5-nitropyridine 140 C5H4N2O3 005418-51-9 4 Abundance Scan 887 (13.387 min): 02721 .D (-) m/z 140.00 100.00% 1-0

5000 .............................................. 441 70 94 108 13.00 13.20 13.40 13.60 13.80 0- i ■ - ■ ■ i • ■ ■ • i > . ... 54 i i | « > » ’ | I | |..... 841........ I................... ‘ ‘ ‘ } i i i rj i +"r i । i H r । j i « J I r r t : j- r i n j r i » 1 ■> TII m/z 70.00 11.37% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #61655: METHYL-2-DEOXY-L-FUCOSIDE 23 39 94 68

5000- 58 112 ■ i 1 ' 13.00 13.20 13.40 13.60 13.80 84 m/z 93.90 10.31% 0i■■ ■•i• ■ • i • ■ i ■ • I 1 ■ • ■ i ■ 1 ■ i • 111'1 i • • i • • ■ ■ i •' ■ i ■ ■ ■ • i miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35384:2-Cyclopenten-1-one, 3-(acetyloxy)- 43

13.00 13.20 13.40 13.60 13.80 5000 m/z 66.10 10.03% 69 140

miz-> 0।<*>*।< 20 30 — 40 1 ■ ■ 50 i ■ 57 Il i 60 • - ■ p 70 80 97

90 100 17 110 120 130 140 TIF

Abundance #35196: Methenamine 42 13.00 13.20 13.40 13.60 13.80 m/z 108.00 9.89%

5000- 140

30 56 71 85 112 98 0‘ TTT ‘ikit *mmmPpt "TI /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

02721.D HP022102.M Fri Mar 01 10:07:52 2002 Page 9

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