GCMS analysis results for sample AD29522, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02FEB01\29522.D Vial: 4 Acq On : 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Disulfide, ethyl 1-methylet... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 13.37 0.04 ug/L 26241 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Disulfide, ethyl 1-methylethyl $... 136 C5H12S2 053966-36-2 7 2 Silane, 2-butenyltrifluoro- 140 C4H7F3S1 055712-74-8 4 3 2-Hydroxy-5-nitropyridine 140 C5H4N2O3 005418-51-9 4 4 2(5H)-Pyridinone, 5-diazo-, mono... 121 C5H3N3O 054459-87-9 4 Abundance Scan 876 (13.375 min): 2S522.D (-) m/z 140.10 100.00% VO

5000-

96 1300 13.20 13.40 13.60 13.80 miz-> 01 ’1141111*1*111151111111 59

20 30 40 50 60 70 80 90 100 110 120 130 140 70 +A1 121 ■ • i1' • • i ■ • ■ ■ i ■ ■ ‘ I m/z 96.10 14.89% Abundance #30728: Disulfide, ethyl 1-methylethyl $$ 2-Methyl-3,4-dit... 43 94 27 66 5000 136 13.00 13.20 13.40 13.60 13.80 m/z 94.10 12.48% 59 35 - 0 ' I " ' ' i ' 4 ' I' TT’6111T*122T 11'1 11 11 mfz~> 20 30 40 50 60 70 80 90 100 110 ‘126 " 130 140 Abundance #35038: Silane, 2-butenyltrifluoro- 55 — -- i ■ ■ 13.00 13.20 13.40 13.60 13.80 5000 140 m/ Z 70.00 11.90% 29 41

85 105 125 93 Of TTT — -4 ‘111 11 ‘ 11 ■'11 ‘ TTT i •— 1111| ■•111111i ‘ ' 1 • ■ I 11 '1 1 ’i. miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance - #35064: 2-Hydroxy-5-nitropyridine VO 13.00 13.20 13.40 13.60 13.80 m/z 121.20 9.68% 5000 66 110 82 93 0 • 11 ■ ■ ■ i ■ ■ ■ ■ i • - i. ■. i.... ।» 111EI ’11/1/IT ’dt TTI • t 1 • 1 * i • ■ m/z—> 20 30 40 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

29522.D SCAN508.M Mon Feb 04 08:41:11 2002 Page 8

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