GCMS analysis results for sample AD29522, Feb 2002

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GCMS analysis report for sample AD29522 listing unknown compounds and surrogate recovery data from February 8, 2002.

NYC-WTC_000036779–000036797

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\29522.D vial: 4 Acq On 1 Feb 2002 1:04 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Silane, [1,2,3-benzenetriyl... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 15.62 0.05 ug/L 27364 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, [1,2,3-benzenetriyltris (... 342 C15H30O3Si3 017864-23-2 10 2 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4Si2 GOOOOO-OO-O 9 3 Morphinan, 7,8-didehydro-4,5-epo... 429 C23H35NO3Si2 055449-66-6 9 4 Bis(trimethylsilyl) derivative o... 429 C23H35NO3S12 000000-00-0 9 Abundance Scan 1073 (15.624 min): 29522.D (-) m/z 73.10 100.00% 73

341 5000 147 429 II" ■ 1 i • ■ ■ • i ' ■ ■1 । 1 1 1 11 1 1 44 15.20 15.40 15.60 15.80 16.00 0+ 1’123. frTTTp-rrrpTprT^^TTTTprrpm-rprrrn- “"1—01191711’338 ■ ■■ ■ i > “ ■ i “. • । “ i “' ■ i m/z 341.00 55.88% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #291363: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 73 239

5000 ■j-T-r-r-r-p-r ‘ ‘ I ‘ ‘ ‘ ‘ I ' ‘ 342 15.20 15.40 15.60 15.80 18.00 45 m/z 429.10 27.77% 133 179 211 O-mp TTTTT TITg apa] mtmmmpmmmm miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #289709: METHYL 2,3-BIS(TRIMETHYLSlLYLOXY)-5-DEUTEROPHENYL.. 73 180 i ■ ■ ■ • i ■ ■ ' 1 I 1 1 1 1 I ' 1 15.20 15.40 15.60 15.80 16.00 5000 m/z 342.00 26.60% 341 45 222 268 310 O-mmmpmmmnpmpm Dg - "’.—211118110—111111111 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #346842: Morphinan, 7,8-didehydro-4,5-epoxy-17-methyl-3,6-... I ' ' ' ' I ' ‘ T-r-p-r-r-r-j-T-r 73 15.20 15.40 15.60 15.80 16.00 m/z 147.00 22.84% 5000’ 146 236 429 196

m/z—> OTTTT TTTT n..,. ।। MLI ....................................... LL 40 60 80 100120140160180200220240260 280300320340 360380 400 420 pr-n-r-p-T 1 ' P ' 1 1 I 1 1 15.20 15.40 15.60 15.80 16.00

29522.D SCAN508.M Mon Feb 04 08:41:11 2002 Page 9

NYC-WTC_000036791

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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