NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02FEB01\31505.D Vial: 6
Acq On : 1 Feb 2002 6:53 pm Operator:
Sample : 508 scan fb Inst : Instrumen
Mise : February 1, 2002 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator)
Title : 508 scan method
Library : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 6 Cyclohexasiloxane, dodecame... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
15.62 0.87 ug/L 510590 Naphthalene-d8 13.19
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91
2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 91
3 2,4-di(trimethylsiloxy)-6,7-(met... 369 C15H23NO6Si2 000000-00-0 64
4 Acetic acid, [bis[(trimethylsily... 356 CllH29O5PSi3 053044-27-2 40
Abundance Scan 1073 (15.624 min): 31505.D (-) m/ z 73.10 100.00%
73
341
5000
147 429
45 15.20 15.40 15.60 15.80 16.00
0-’ 1’I 4411I
117
TTTTTT
179 . 207 251 281 311 | |
T——CPuguB)mmga) "....‘ r397 ...... l m/ z 341.00 58.31%
■" i" " r ‘7 ■ i ■
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc...
73 341
429 ......................... /.....................
5000
15.20 15.40 15.60 15.80 16.00
147
m/z 429.20 22.77%
m/z->
0- " i ■" ■ i" “I i1"11 ■ ■"i1 ■
117
+L 207 267 311
1’21111011111110110111001110111371111111111111 "mmmTT
40 60 80 100120140160180200220240260280300320340360380400420
Abundance #352522: Cyclohexasiloxane, dodecamethyl-
73
/
15.20 15.40 15.60 15.80 16.00
5000 341
m/z 147.10 20.29%
429
147
, I 207 271 311 I |
0 ...... I' !'''' I ■ " ' I" " I !1 . .......... 1 ii 11 ] i ■ 11111111 ill ■ 111111111 n 11 .. ....... 11' [1' " I'1'' I'1111'
n/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #312619: 2,4-di(trimethylsiloxy)-6,7-(methylenedioxy)-2H-1... i ■ ■ ■ ■ i 1 ■ ' ■ i ■ r 1 1 i ■ '
208 251
34.1 15.20 15.40 15.60 15.80 16.00
310 m/z 342.00 18.47%
5000
369
163
0 "’9UT’’0"B11111101111191110110000310111111 "i"1 I........| TT H ft ■ |' ’ " ! " " I' ■H _ —_
iz-> 40 60 80 100120140160180200 220240260280300320340360380400420 15.20 15.40 15.60 15.80 16.00
31505.D SCAN508.M Mon Feb 04 10:14:22 2002 Page 8
NYC-WTC_000004139
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