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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010537–000010557

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\030402\2335.D Vial: 7 •Acq On 4 Mar 2002 3:11 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 8.935 642 646 652 rVB 68692 133582 1.28% 0.209% 2 9.579 711 717 737 rBV 3039546 7284867 70.04% 11.388% 3 12.083 988 993 1002 rVB 536207 880801 8.47% 1.377% 4 13.053 1094 1100 1115 rBV 4954854 9484177 91.18% 14.826% 5 15.139 1325 1330 1335 rBV2 908480 1509130 14.51% 2.359%

6 15.983 1418 1423 1429 rBV 82199 139313 1.34% 0.218% 7 17.879 1627 1632 1637 rVB 633351 1128211 10.85% 1.764% 8 18.169 1657 1664 1676 rBV 5313616 10284849 98.88% 16.077% 9 18.795 1729 1733 1743 rBV 155220 287204 2.76% 0.449% 10 20.309 1895 1900 1906 rBV 517294 898144 8.64% 1.404%

11 22.414 2127 2132 2137 rBB2 402817 716845 6.89% 1.121% 12 22.532 2137 2145 2157 rBV2 4522530 10401191 100.00% 16.259% 13 22.677 2157 2161 2173 rVB2 37009 118205 1.14% 0.185% 14 24.291 2334 2339 2344 rBB 315971 538184 5.17% 0.841% 15 26.005 2522 2528 2535 rBB 226059 448194 4.31% 0.701%

16 27.457 2684 2688 2694 rBV 639918 1169863 11.25% 1.829% 17 27.556 2694 2699 2707 rVB 224951 448562 4.31% 0.701% 18 28.990 2852 2857 2868 rBV 187854 418237 4.02% 0.654% 19 30.341 2998 3006 3025 rBV2 4276124 10238613 98.44% 16.005% 20 31.629 3142 3148 3161 rBV 116640 311695 3.00% 0.487%

21 32.826 3274 3280 3294 rBV2 83353 230837 2.22% 0.361% 22 33.933 3396 3402 3410 rBV 55221 153119 1.47% 0.239% 23 34.214 3425 3433 3449 rBV2 2746776 6618136 63.63% 10.345% 24 34.985 3512 3518 3527 rBV2 41873 129691 1.25% 0.203%

Sum of corrected areas: 63971650

2335.D 5080302.M Mon Mar 18 08:31:16 2002 Page 1

NYC-WTC_000010542

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NYC-WTC_000010542Source: NYC Law Department, mirrored locally

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