GCMS analysis results, sample AE00893, Feb 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report 2 Data File : C:\HPCHEM\l\DATA\FEB1102\893.D Vial: 42 Acq On : 13 Feb 2002 4:02 am Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Butanamine, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.35 ug/1 25993 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 5 2 1 - Pent anamine 87 C5H13N 000110-58-7 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 4 Silane,tetramethyl-__ 88 C4H12Si 000075-76-3 4 Abundance Scan 347 (8.226 min): 893.D (-) m/z 73.00 100.00% 73

5000 43

39 55 69, 7.80 8.00 8.20 8.40 8.60 mm tmmmmpm .............. ............. ..

_M ।....।....i. >।.11.. m/z 43.05 42.93% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #766:1-Butanamine, 2-methyl- 30

5000 7.80 8.00 8.20 8.40 8.60 m/z 41.05 16.74% .... 15........27 56 ,4144 87 I l i J | ! I I I | I I T i |'! ! .. । .. >. j 111.|.... 11. i. 111.. 11 M . 1. i n ।. 1 ■. । ■.. > ।.. m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance *776; :-Pertanamind 30 1*’1*[’1-I* 6rfI8 18** 7.80 8.00 8.20 8.40 8.60 5000 m/z 45.05 15.75%

15 27 3841 45 55 87 TBT1’115mTTpau"npmppEmT mfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62884:1-Butanamine, 3-methyl- 30 7.80 8.00 8.20 8.40 8.60 m/z 39.0,5 8.46% 5000-

27 4144 55 59 70 73 87 ■ ■ 11" “ i ■ ‘ “ i “ • > i'1'1 1 ‘" i “ ‘ ‘ i11111' “ ‘ i ‘' * 11 “11 “ “ I I >"111' “ I"'11111' I" “ 11' IT * ■ i ■ • 1 1 i ■ ' ■ ■ i • 1 • ■ i ■ m/z->....5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 [ 7.80 8.00 8.20 8.40 8.60

893.D GCMS0208.M Wed Feb 20 09:49:07 2002 Page 1

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