GCMS sample results, AE00899, Feb 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\FEB1102\899.D Vial: 34 Acq On : 12 Feb 2002 8:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Butanamine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

47.90 0.57 ug/1 27596 Perylene-dl2 38.11 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Butanamine 73 C4H11N 013952-84-6 3 2 Carbon dioxide 44 CO2 000124-38-9 3 3 Nitrous/Oxide 44 N20 010024-97-2 3 _ 4 Ethyne/; fluoro- \____ 44 C2HF 002713-09-9 2 Abundance s N Scan 4668 (47.898 min): 899.5 (-) m/z 39.95 100.00% U V 5000

73 209 47.60 47.80 48.00 1 ' r1 1 1 1 r' ■ ■ i ■ ■ ■ ■ i • ‘ ‘ i ■ ' 1 ' i 1 ' ‘ ' i ' 1 ‘ ■ i ■ ■ ■ ‘ i ‘ ' ■ i ■ ' ■ m/z 43.95 51.03% m/z-> 20 40 _ 60 80 100 120 140 160 180 200 Abundance #296: 2-Butanamine 44

5000 47.60 47.80 48.00 m/z 35.90 0.80% 15 30 58 1 .1 72 • 1 1 ■ ■ 1 ' i ■ ' ' • i • ‘ ‘ ■ i ' ' 1 ' i ' ' ‘ ■ i ‘ ■ • ■ i ‘ ‘ ‘ ■ i ' ‘ • ■ • i • ■ ■ ■ i ' miz-2________ 20.... 40 60...80 100 120. 140 160__ 180 200 Abundance tod; Ceron pi 44 _________ 47.60 47.80 48.00 5000 m/z 44.95 0.64%

16 ' ' i ' ‘ 1 ' i ’ ■ • ‘ i ‘ 1 ’ ’ i ’ 1 ' 1 i 1 1 ‘ 1 i 1 1 1 1 ( 1 1 1 ■ i ■ ■ ■ ' i ■ ‘ 1 1 i ■ 1 m/z--> 20 40 60 80 100 120 140 160 180 200 Abundance #39: Nitrous Oxide 44 47.60 47.80 48.00 m/z 48.90 0.60% 5000 30 14 -p— I II nilII ■ ■ i • • ■ ■ i 1 ■ ■ 1 i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 1 • ■ i ■ ' m/z~> 20 40 60 80 100 120 140 160 180 200 47.60 47.80 48.00

899.D GCMS0208.M Wed Feb 20 09:53:26 2002 Page 3

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