GCMS analysis results for sample AE03247, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.

NYC-WTC_000006126–000006145

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document ocaiL.il tpOuU KCDOL L

Data File : C:\MSDCHEM\1\5973N\02MAR01\03247.D Vial: 2 Acq On : 1 Mar 2002 4:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L

Peak Number 7 3-Pentanol, 2,4-dimethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.42 ug/L 1550290 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-633 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 Abundance Scan 223 (5.891 min): 03247. D (-) m/ z 73.10 100.00% 70 ......... |

5000 43 5.60 5.80 6.00 6.20 o ■ 11 ■ ■ ■ ■ i > ■ ■ > i ■ । 1155 , 87 103 1 1 1 1 ' ' 1 1 '" I 1 1 1 'T' “ I ‘IWIIG m/z 43.10 23.00% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17063: 3-Pentanol, 2,4-dimethyl- 70

5000 55 5.60 5.80 6.00 6.20 43 m/z 41.10 9.51% 27 15 m/z-> 11 04 '' r ' " i' " 11' ‘ " i' 4 1111110111111111110/111——110701T1Tm9111’-1-’’11U 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70 ' ' PIP । 4 ■ Mmin M 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.18% 43

miz-> 0 Tp 11’211111/113 ,i 27 + 87 "''I ""I ""I 11355 174 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 11" " i'1" i ■' " i " " r "' i11 ■ ■ i ■

Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70 5.60 5.80 6.00 6.20 m/z 71.00 6.48%

5000 43 55 27 87 113 174 0 TTTpr ' i " ■' i " '1, 1i 1 "''I"" . .. . ■ r ■ ‘' i " ■' I " 111" " I " " 1111111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

33247.D HP022102.M Mon Mar 04 12:33:21 2002 Page 9

NYC-WTC_000006138

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