GCMS analysis results for sample AE03247, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.

NYC-WTC_000006126–000006145

Folder label: “GCMS X 2/12/02 A 3/01/02”

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Data File : C:\MSDCHEM\1\5973N\02MAR01\03247.D Vial: 2 ' Acq On : 1 Mar 2002 4:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiple: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 2-Butenoic acid, 2-methoxy-... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. 5.02 0.08 ug/L 37522 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butenoic acid, 2-methoxy-, met... 130 C6H10O3 056009-29-1 33 2 6-Undecanone (CAS) $$ DI-N-AMYL ... 170 C11H220 000927-49-1 9 3 E-2-hexenyl butanoate $$ TRANS-2... 170 C10H18O2 000000-00-0 9 4 2-Nitro-l-propanol $$ 2-Nitropro... 105 C3H7NO3 002902-96-7 9 Abundance Scan 146 (5.022 min): 03247.D (-) m/ z 71.00 100.00% 43 71

5000 59 — 207 1 1 04 1 4.60 4.80 5.00 5.20 5.40

miz-> 0- ■ ।111' ।' M :20 30 40 50 60 70 80 90 100110120130140150 160170180 190 200 210 m/ Z 43.10 99.83%

Abundances #26065:2-Butenoic acid, 2-methoxy-, methyl ester, (E)- 43 71

5000 27 1 MWAyw VAA, NA i1■'■i1■■ii11'1i1,11t11 4.60 4.80 5.00 5.20 5.40 57 m/z 41.10 76.49% 130 0 11111111211011111-11100001—B0I0—00I01-"TB1E111111011710111m11111UUTTTC ——P1UI1T’21’01011 /z-> 20 30 40 50 60 70 80 90 100110 120130140150160170180190 200 210 Abundance #74204: 6-Undecanone (CAS) $$ DI-N-AMYL KETONE $$ Amyl ket... 43 71

4.60 N 4.80 5.00 5.20 5.40 58 m/z 69.10 39.39% 5000 27 85 99

miz—> 0 HH I" " i i'" 1' i"111" " r1" i" " i" " i 20 30 40 50 60 70 80 90 100110120130140150160170 180 190 200 210 i " " i" " i" " i ■ ■ ‘' r ■" i ■"r i'"

Abundance #73708: E-2-hexenyl butanoate $$ TRANS-2-HEXENYL BUTANOATE 71 4.60 4.80 5.00 5.20 5.40 41 m/z 59.10 29.48%

5000 27 82 54

m/z-> 0 ... || — ''" I I— l......... ■ ■ ■ ।1 ■ ■ ■ । 128 i " ■11"'11 ■ ■" i" " r1" I" 170 I"111" " I "111"1111" n... A. 20 30 40 50 60 70 80 90 100110 120130140150 160170 180 190 200 210 4.60 5.20 5.40

)3247.D HP022102.M Mon Mar 04 12:33:21 2002 Page 8

NYC-WTC_000006137

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