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GCMS analysis results for sample AE03247, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.

NYC-WTC_000006126–000006145

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006139
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document ulpraLY bearcr compound Keporc

Data File : C: \MSDCHEM\1\5973N\02MAR01\03247.D Vial: 2 Acq On : 1 Mar 2002 4:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 6.09 0.11 ug/L 51163 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 64 2 3-Methylpyrrolidin-3-ol 101 C5H11NO 000000-00-0 9 3 1,2-DIETHYLDIBORANE-D4 88 C4H10D4B2 000000-00-09 4 ACETOFLUORONITRILE $$METHYLFLUO. . . 59 C2H2FN 000503-20-8 5 Abundance Scan 241 (6.095 min): 03247.D (-) m/ z 43.10 100.00% 43

59 5000 101 - PT . 4 . IRO . — । - , — 49 5,80 6.00 6.20 6.40 84 59.00 0 P TrTTTr^nTm*1Tm^^^ '" 11"111' “ 111" I' m/ z 50.39% mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #16599: 2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 40

59 4./.... 5000 5.80 6.00 6.20 6.40 101 m/z 58.10 23.08% 31 0 mm TH 83 112 |■*<<। -1111' । ।।' 111', 111 ■ ■ >. ।. 1111111 TETIug n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #8924:3-Methylpyrrolidin-3-ol 50 42 5.80 6.00 6.20 6.40 5000 101 m/ z 101.10 21.90%

0 " I'''' I'" ‘ 11"' 11'" I' TT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #3192:1.2-DIETHYLDIBORANE-D4 41 5.80 6.00 6.20 6.40 m/z 56.00 10.45% 59 5000 27 0 54 n/z-> 0- ■' I"111 +HMARH4L 35 m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 5.80 6.00 6.20 6.40

93247.D HP022102.M Mon Mar 04 12:33:21 2002 Page 10

NYC-WTC_000006139

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NYC-WTC_000006139Source: NYC Law Department, mirrored locally

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