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GCMS analysis results for sample AE03014, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE03014 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005698–000005706

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\3014.D Vial: 38 Acq On 9 Feb 2002 9:15 pm Operator: 209 GALOS Sample GC/MS SCAN "2.11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.217 341 346 362 rBV 146273 332132 7.74% 1.502% 2 12.348 790 796 811 rVB 1449166 3084532 71.92% 13.946% 3 15.993 1186 1193 1210 rBV 1975570 3912171 91.22% 17.688% 4 21.308 1765 1772 1793 rBV 2119295 4288716 100.00% 19.391% 5 25.761 2250 2257 2267 rBV 1998002 4223488 98.48% 19.096%

6 30.828 2804 2809 2816 rBV 235736 458050 10.68% 2.071% 7 33.830 3128 3136 3150 rBV 1475714 3333131 77.72% 15.070% 8 38.117 3593 3603 3620 rBV2 830499 2485145 57.95% 11.236%

Sum of corrected areas: 22117365

3014.D GCMS0208.M Wed Feb 13 11:13:18 2002

NYC-WTC_000005703

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NYC-WTC_000005703Source: NYC Law Department, mirrored locally

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