GCMS analysis results for sample AE02711, Mar 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0 7 02\2 711.D Vial: 22 Acq On 8 Mar 2002 10:23 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-(2-Carboxyvinyl)pyridine, tr Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.46 0.63 ug/1 104609 Chrysene-dl2 33.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-(2-Carbo: inyl) pyridine, trans 149 C8H7N02 007340-22-9 45 2 2 -Acetylbenzoic acid 164 C9H803 000577-56-0 36 3 Ethanone-; 2-(formyloxy)-1-phenyl- 164 C9H803 055153-12-3 35 4 1-Propanone, 2,2-dichloro-3-hydroxy 218 C9H8C12O2 054824-08-7 25 Abundance Scan 3095(33.456 min): 2711.D (-) 105 ] m/z. 104.95 100.00% 149

5000 77

51 70 ____ 33.20 33.40 33.60 33.80 39 | , 163 i■■■■i■■11 I' 1 1 1 I1 '1 11' -IPPTT - I 1 ' 1 1 I 1,1 1 1 I m/z 149.00 82.33% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #9445: 2-(2-Carboxyvinyl)pyridine, trans 104 149

5000 _ 33.20 33.40 33.60 33.80 51 79 m/z 77.00 38.96% ........ । । I...... i i | I I । । i'i-n-1 | i i i i । > i- m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance : ■ ■ 149 . 4. , m/z 33.20 33.40 33.60 33.80 51.00 10.21%

.„ 5000

50 65 77 93 105 121 .................................... 164 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #13369: Ethanone, 2-(formyloxy)-1-phenyl- TTr 1 ' । ■ ■ ■ 1 11 1 1 r A 105 33.20 33.40 33.60 33.80 m/z 106.00 . 88% 5000 77

51 31 - mmPP 164 ... 1 m । m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 33.20 33.40 33.60 33.80

2711.D GCMS0208.M Wed Mar 13 15:00:40 2002 Page 3

NYC-WTC_000005482