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GCMS analysis results for sample AE02597, Mar 2002

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Laboratory report documenting GCMS analysis of sample AE02597 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005281–000005290

Folder label: “GCMS X 2/5/02 A 3/1/02

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(QT Reviewed) Nvc om Pubic Portal Document iation Report Quantitation Report (QT Reviewed) A ■

de C:\HPCHEM\1\DATA\MARO1O2\2597.D Vial: 7 2 1 Mar 2002 2:15 pm Operator: ES ie gc/ms scan 2/5 Inst : GC/MS 209 Multiplr: 1.00 Integration Params: GOOFY.P ant Time: Mar 4 11:19 2002 Quant Results File: GCMS0208.RES

mt Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) le : 209 625/TCLP calibration table t Update : Wed Feb 27 11:30:15 2002 oonse via : Initial Calibration aAcq Meth : GCMS0208

al Standards R.T. Qlon Response Cone Units Dev(Min)

,4-Dichlorobenzene-d4 12.32 152 294011 20.00 ug/1 -0.03 aphthalene-d8 15.95 136 1142564 20.00 ug/1 -0.04 enaphthene - dl 0 21.27 164 607319 20.00 ug/1 -0.04 tenant hrene - dl 0 25.71 188 890538 20.00 ug/1 -0.05 rysene-dl2 33.78 240 623672 20.00 ug/1 -0.06 rylene-dl2 38.05 264 430889 20.00 ug/1 -0.07

onitoring Compounds i-DDD 30.80 235 56371 6.06 ug/mL 0.30 I Amount 5.000 Recovery = 121.20%

ompounds Qvalue . itroso-dimethyl amine 0.00 74 0 N.D. (2-Chloroethyl)ether 0.00 93 - 0 N.D. Dichlorobenzene 0.00 146 0 N.D. Dichlorobenzene 0.00 146 0 N.D. Dichlorobenzene 0.00 146 0 N.D. -oxybis(1-Chloropropan 0.00 45 0 N.D. roso-di-n-propylamine 0.00 70 0 N.D. 'hloroethane 0.00 117 0 N.D. benzene 0.00 77 0 N.D. crone 0.00 82 0 N.D. -Chloroethoxy)methane 0.00 93 0 N.D. ■Trichlorobenzene 0.00 180 0 N.D. .alene 0.00 128 0 N.D. lorobutadiene 0.00 225 0 N.D. lorocyclopentadiene 0.00 237 0 N.D. conaphthalene 0.00 162 0 N.D. lphthalate 0.00 163 0 N.D. itrotoluene 0.00 165 0 N.D. thylene 0.00 152 0 N.D. thene 0.00 153 0 N.D. itrotoluene 0.00 165 0 N.D. hthalate 22.75 149 450 N.D. phenyl-phenylether 0.00 204 0 N.D. 0.00 166 0 N.D. page 2 1/ 1,2-Diphenylhyd 0.00 77 0 N.D.

r out of range (m) = manual integration ’8.M Mon Mar 04 11:20:44 2002 v

NYC-WTC_000005283

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NYC-WTC_000005283Source: NYC Law Department, mirrored locally

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