GCMS analysis results for sample AD31129, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB 0802\31129.D Vial: 13 Acq On 8 Feb 2002 9:00 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Glycine, methyl ester Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.27 0.37 ug/1 34161 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Glycine, thyl ester 89 C3H7NO2 000616-34-2 42 2 Methanethioamide, N,N-dimethyl- 89 C3H7NS 000758-16-7 42 3 1,3-Dioxane 88 C4H802 000505-22-6 10 4 2-Propenenitrile, 2-chloro- 87 C3H2C1N 000920-37-6 9 Abundance Scan 133 (6.267 min): 31129.D (-) m/ z 87.10.. 100.00% 87 43 55 5000

___ 6.00 6.20 6.40 6.60 103

m/z-> +49 I I 35 I II TTTUTIWTNTTWTTTTTTNTTTTTTT) 71 il■ ....... I■ ■ ■ । ■ ■ ■ ■ 11111|l ।

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 m/ z 89.00 94.38% 111111 TTpT-l-rp-rrq-

Abundance #870: Glycine, methyl ester 89

5000 —PPTTPTTTPP 6.00 6.20 6.40 6.60 44 59 m/z 43.05 72.27% 66 i - ■ ■ 54 , । > i111 ■ i m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance ' . 89 —Am—AA—n ‘6.00 1 6.20 6.40 6.60 __ 5000 m/ z 55.00 5 0.87%

42 74 33 47 56 ’ ’I’’’’I’’’’I’A’I’’A’A’S’**d’OdAIIGGG*GG|IIVSTV/I| m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #62910: 1,3-Dioxane ............................................ 87 6.00 6.20 6.40 6.60 m/z 45.05 2 0.08% 5000 31

58 17 26 | 41 ill 1'1"I""111' i ■"i -mmmmmm i■i ।।।■i ■ *' m/z—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 6.00 6.20 6.40 6.60

31129.D GCMS0208.M Mon Feb 11 12:30:56 2002 Page 1

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