GCMS analysis results, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB0802\31586.D Vial: 7 Acq On : 8 Feb 2002 3:09 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Glycine, methyl ester Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.28 0.35 ug/1 36411 1,4-Dichlorobenzene-d4 12.35

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Glycine, methyl ester 89 C3H7NO2 000616-34-2 42 2 Methanethibamide, N,N-dimethyl- 89 C3H7NS 000758-16-7 42 3 1-Butanamine, N-methyl-N-nitro- 132 C5H12N202 052330-07-1 36 4 Acetamide N-ethyl- 87 C4H9NO 000625-50-3 9 Abundance Scan 134 (6.276 min :31586.D (-) ' m/z 89.00 100.00% 89 43 55 5000

103 1 ‘ ■ ■ i 17 1 1 1 1171 11 1 ■ i 1 1

m/z-> 20 —4l30 40 49 I i I > 1 ' i 1 ' 50 I1'1..... 70 60 70 80 lm 90 100 110 120 130 ___ 6.00 m/z 6.20 87.1,0 6.40 6.60 97.01% Abundance #870: Glycine, methyl ester 89

5000 A.. p .I I | I I I ! ___ 6.00 6.20 6.40 6.60 __ 44 m/z 43.05 78.71% , 59 m/z-> 20 ....... 30 Il'...... 40 50 160 6670......... 80 FTTEE—uuuumummTTOTT !90 100 110 120 130 Abundance 89 MuIgi 6.00 6.20 6.40 6.60 , 5000 m/z 55.00 64.21% 42 74 33 56 1 1 | 1 1 ‘ 1 1 1 1 1 1 1.............. . | | I I I | I , I !'| I I I I | ! I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5724:1-Butanamine, N-methyl-N-nitro- A A.... "N", ■ 43 89 _ 6-00 6.20 6.40 6.60___ m/z 45.05 23.32% 5000

30 —.... —l. ... 1. 132 ’I’*t*d*’II+III**IIIIIII A.A.. m/z-> 20 30 40 50 60 70 80 !90 100110 120 130 £ 6.00 6.20 6.40 6.60

31586.D GCMS0208.M Mon Feb 11 12:33:06 2002 Page 1

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