GCMS analysis results for sample AE02712, Mar 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0702\2712.D Vial: 23 Acq On 8 Mar 2002 11:22 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Butanamine, N-methyl-N-nitro Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.23 0.54 ug/1 56657 1,4-Dichlorobenzene-d4 12.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanamine, N-methyl-N-nitro- 132 C5H12N202 052330-07-1 36 2 Methanethioamide, N,N-dimethyl- 89 C3H7NS 000758-16-7 33 3 1,3-Dioxane 88 C4H802 000505-22-6 9 4 Disulfide, methyl 1-methyl-l-(methy 168 C5H12S3 069078-84-8 9 Abundance............./............... Scan 129 (6.229 min): 2712.D (-) m/ z 87.10100.00% 87 43 55 5000

103 AM WAA 5.80 6.00 6.20 6.40 6.60

._N ...... .......... rJ.I.,'.*.... /I......Il 1 i ■ ' ' 1 i 1 ' ' 1 i ' ■ ' ' i 1 ' ■ ■ I ' 1 ' ' i m/ z 89.00 98.51% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5724: 1-Butanamine, N-methyl-N-nitro- 43 89

5000 --A 6.20 5.80 6.00 6.40 6.60 m/z;

N 43.05 68.57% 30

m/z-> 1 I ' ' ' ' I ' ' ' ' I ' 10 20 30 ' I 1 40 50 7.... 73 60 70 ‘ i ■ ■ I' I > 1 ■ ■ । ■ • ■ • । • • ■ ■ । ’ 80 90 100 110 120 132 'I 1 1 1 1 I 130 Abundance 89 [dnil 5.80 MwWA 6.00 6.20 6.40 6.60 5000- m/ z 55.00 57.96%

42 74 33 56 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #62910: 1,3-Dioxane A. 87 5.80 6.00 6.20 6.40 6.60 m/z 41.05 28.69% 5000 31

58 41 17 m/z-> ■ i ' ■ ' ■ i ■ .... 'll.............. 1 i ' ‘ ' ■ i 1 ■ ' ' i r ' ' 1 1 1 1 1 ' I 1 1 1 1 I 10 20 30 40 50 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40 6.60

2712.D GCMS0208.M Wed Mar 13 15:01:36 2002 Page 1

NYC-WTC_000005491