GCMS analysis results for sample AD31255, Feb 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ FEB14 02\31255.D Vial: 28 Acq On : 15 Feb 2002 5:23 am Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 Methanethioamide, N,N-dimethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.27 0.29 ug/1 35177 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methanethioamide, N,N-dimethyl- 89 C3H7NS 000758-16-7 53 2 Glycine, methyl ester 89 C3H7NO2 000616-34-2 38 3 1-Butanamine, N-methyl-N-nitro- 132 C5H12N202 052330-07-1 36 4 Butanoic acid, butyl ester 144 C8H1602 000109-21-7 36 Abundance Scan 133 (6.266 min): 31255.D (-) m/z 89.00 100.00% 43 89

55 5000 - 103 6.00 6.20 6.40 6.60

miz-> -41499+ 20 30 40 50 60 i I

70 71

80 90 100 110 ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ 1 1 ■ i ' ‘ 120 130 • i m/z 87.10 96.74% Abundance #871: Methanethioamide, N,N-dimethyl- 89

5000 -PPP 6.00 6.20 6.40 6.60T 42 74 m/z 43.05 95.80% I miz-> ... 3?. 20 ' ' '30 ‘ ' 40 | |l,., , ■ 50 60 ..70080 । i ‘ !90 100 110 * 120 130 Abundance #870: Glycine, methyl ester 89 -A-- 6.00 6.20 6.40 6.60 5000 52.53% 44 59 T-r-p-r-n-p -------------------- miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5724: 1-Butanamine, N-methyl-N-nitro- 43 89 6.00 6.20 6.40 6.60 m/z 44.95 22.49% 5000

30 57 . 132 m/z-> 20 30 40 ...... . 10 •la11****1***1** 50 60 70 80 90 100 110 120 130 6.00 6.20 6.40 6.60

31255.D GCMS0208.M Fri Feb 15 14:04:19 2002 Page 1

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