GCMS analysis results for sample AD31252, Feb 2002

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Laboratory report documenting GCMS analysis of sample AD31252 conducted on February 11, 2002, including surrogate recovery data.

NYC-WTC_000005210–000005218

Folder label: “GCMS X 2/4/02 A 2/8/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\l\DATA\FEB0802\31252.D Vial: 12 Acq On 8 Feb 2002 8:02 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Glycine, methyl ester Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.27 0.34 ug/1 32084 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Glycine, methyl ester 89 C3H7NO2 000616-34-2 59 2 Methanethioamide, N,N-dimethyl- 89 C3H7NS 000758-16-7 36 3 1,3-Dioxane 88 C4H802 000505-22-6 9 4 Ethane, /isothiocyanato- 87 C3H5NS 000542-85-8 9 Abundance Scan 133 (6.268 min): 31252.D (-) i m/z 87.10 100.00% 87 43 55 5000

___6.00 6.20 6.40 6.60__ 103

mz-> I'1111 mm 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 m/z 89.00 96.02% Abundance #870: Glycine, methyl ester 89

5000 1 ) । । । । । । । 6.00 6.20 6.40 6.60 44 59 ‘ m/z 43.05 68.76% 1 54 66 i, ’ I’14+1’’’*A’’t’I’*’’1’Bd’I’4**1—2**1’4**1**’}—29"B—B—WB-I—B9IIBVIIBS|- ITiTTrp ri 11111111111111 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance • ■ . ; ■ 89 A.. A, 6.00 6.20 VW A______ ■ 11,V1 1 r • 1 ’ ■ 6.40__ 6.60___ 5000 m/z 55.00। 60.70%

42 _ 74 33 47 56 " I1"' p 1" I" " I"1' I" " 1 TWWImmummgn । ■ i ■■■>i■> ■ ■ । ■ ■ ■ ■ ।"111" " I"1111" m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #62910: 1,3-Dioxane AA / ________ ' ' U’ । . . . . । . I I’I r i -I |-> i ! i 87 6.00 6.20 6.40 6.60 m/z 44.95 17.78% 5000 31

m/z-> 17 26 41 Hi TTT ।' ■" ।11 ■ i'1' । ■' ■ ■ ।1 ‘ ■11r 1" । ■ ■" ।'1111 ‘" ■ ।111' । ■1111111111111111111111111111111'1111'11 I....... LI.......... 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 6.00 6.20 6.40 6.60 J

31252 .D GCMS0208.M Mon Feb 11 12:32:29 2002 Page 1

NYC-WTC_000005217

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