Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\JAN2502\30651.D Vial: 35 Acq On : 25 Jan 2002 10:53 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 16
R.T. EstConc Area Relative to ISTD R.T.
10.96 0.37 ug/1 270971 1,4-Dichlorobenzene-d4 11.48
Hit# of 5 Tentative ID MW Mol Fo 22m CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 86 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 47 3 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance Scan 644 (10.959 min): 30651.D (-) m/z 281. 0.0 100.00% 201
5000
45 59 73 85 103 119 133 147 165177 113 207 24 249 265 10.60 10.80 11.00 11.20
m/z-> ■' 1''1 ■ '"i'' ■111 ri 1 IT 40 60 1111111''11 rY ■1 drth । t’Pi 11 r 80 100 120 140 160 180 200 220 23240 5 .h —iTTTT 260 280 m/z 282.00 28.37% Abundance #72646: Cyclotetrasiloxane, octamethyl- 281
5000- 11 TIT 10.60 10.80 11.00 11.20 265 m/z 283.00 16.79% 45 59 73 133 177 193 207 235 111/‘t1111111112111111111111112111111111*111m1m11—EI11ITII0OI1‘ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-pheny-4-(2-cyano-2-phenyietheny) 1 281
10.60 10.80 11.00 11.20 " 1' 5000 m/z 192.90 12.75% 2 253 126 293 , 266 t 224 240 1 m/z-> 40 60 80 100 '120' 140 160 180 2Oo' '220' 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 10.60 10.80 11.00 11.20 ' ' ' ' m/z 190.90 11.73% 5000
102 123 141 175 204 247 ■ ■ i 1 ■ 1 ' I 1 ' ' 1 i ' ' ' ' i 1 ' ■ ‘ I ' 1 ' ' i ' ' 1 ' i ■ ' 1 1 1 1 1 1 1 11 ' TIIPPPPPTPTTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.60 10.80 11.00 11.20
30651.D GCMS1126.M Mon Jan 28 12:23:06 2002 Page 2
NYC-WTC_000004222
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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