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Toxaphene analysis results for samples TOXC1-3, Dec 2001

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Chemical analysis report listing toxaphene compound concentrations and surrogate recovery metrics from December 2001.

NYC-WTC_000089559–000089567

Folder label: “508 X 11/27/01 A 12/4-12/26/01

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NYC 9/11 Public Portal Document

Response Factor Report Instrumen

Method : C:\MSDCHEM\1\METHODS\011224T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Wed Dec 26 10:40:08 2001

Calibration Files 1 =TOXC1.D 2 =T0XC2.D 3 =T0XC3.D

Compound 1 2 3 Avg %RSD

1) Toxaphene Peak 1 4.628 4.735 4.872 4.745 E7 2.58 2) Toxaphene Peak 2 8.370 8.490 8.468 8.443 E7 0.76 3) Toxaphene Peak 3 5.210 4.651 4.657 4.839 E7 6.64 4) Toxaphene Peak 4 1.791 1.942 1.964 1.899 E8 4.97 5) Toxaphene Peak 5 6.807 7.6'88 8.440 7.645 E7 10.69 6) s 2,4-DDD SURROGATE 3.921 3.957 4.157 4.012 E9 3.17 Signal #2 Calibration Files 1 =TOXC1.D 2 =T0XC2.D 3 =T0XC3.D

Compound 1 2 3 Avg %RSD

1) Toxaphene Peak 1 2.284 2.274 2.257 2.272 E7 0.60 2) Toxaphene Peak 2 1.005 1.140 1.188 1.111 E8 ' 8.56 3) Toxaphene Peak 3 3.770 3.690 3.807 3.755 E7 1.59 4) Toxaphene Peak 4 1.030 1.088 1.120 1.079 E8 4.19 5) Toxaphene Peak 5 1.172 1.252 1.329 1.251 E8 6.26 6) s 2,4-DDD SURROGATE 2.858 2.560 2.528 2.649 E9 6.87

(#) = Out of Range 011224T.M Mon Dec 31 15:22:13 2001 Page 1

NYC-WTC_000089559

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NYC-WTC_000089559Source: NYC Law Department, mirrored locally

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