NYC Law Department release
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← Document results/DEP Box 68/508 X 11/13/01 A 12/7/01
Document / 2 pages

Pesticide spike recovery data, Dec 2001

Machine-extracted title · confidence 95%

Quality control record showing pesticide spike recovery rates and compound responses from testing conducted in December 2001.

NYC-WTC_000090016–000090017

Folder label: “508 X 11/13/01 A 12/7/01

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Scanned page image, NYC-WTC_000090016
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\5O8\O112O7\1113REFT.D\ECD1A.CH Vial: 18 Signal #2 : C:\MSDCHEM\l\DATA\508\011207\1113REFT.D\ECD2B.CH Acq On : 07 Dec 2001 10:31 pm Operator: Nefliu Sample : 11/13 ref tox Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 20 15:39:31 2001 Quant Results File: 011207T.RES

Quant Method : C:\MSDCHEM\1\METHODS\011207T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Mon Dec 17 14:03:38 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.46 15.05 494.0E6 374.3E6 0.152m 0.163 Spiked Amount 0.200 Recovery 76.00% 81.50%

Target Compounds 1) Toxaphene Peak 1 14.88 15.78 12201824 8015408 0.237m 0.410m# 2) Toxaphene Peak 2 15.23 16.20 21055200 26031387 0.305m 0.275m 3) Toxaphene Peak 3 15.66 16.36 24513661 5494986 0.640m 0.181m# 4) Toxaphene Peak 4 17.31 16.78 20123663 18707224 0.128m 0.204m# 5) Toxaphene Peak 5 17.64 17.86 5242560 15430340 0.090m 0.139 #

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1113REFT.D ■ 011207T.M Thu Dec 20 15:40:57 2001 Page 1

NYC-WTC_000090016

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NYC-WTC_000090016Source: NYC Law Department, mirrored locally

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