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Document / 6 pages

Pesticide chromatographic data review, Dec 2001

Machine-extracted title · confidence 90%

Review of chromatographic signals and compound quantification data for pesticide analysis conducted in December 2001.

NYC-WTC_000092401–000092406

Folder label: “508 X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\5O8\O112O1\2PESTC1.D\ECD1A.CH Vial: 21 Signal #2 : C:\MSDCHEM\l\DATA\508\011201\2PESTCl.D\ECD2B.CH Acq On : 03 Dec 2001 9:56 am Operator: Nefliu Sample : pest ccvl Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 12 11:18:16 2001 Quant Results File: 011203P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011203P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 03 10:48:55 2001 Response via : Initial Calibration DataAcq Meth : 508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds

Target Compounds 1) Propachlor 9.18 8.60 19367320 12091664 0.046m(ff/. 0.037 2) g-BHC 9.95 10.27 364.2E6 258.1E6 0.055 q/y. 0.045 3) Heptachlor 11.12 11.32 102.1E6 61277253 0.018^f/. 0.015 4) Aldrin 11.82 12.06 147.4E6 121.9E6 0.024iMy. 0.021 5) Heptachlor Epoxi 13.26 13.41 267.3E6 216.6E6 0.049 ItfL'/- 0.043 6) 4,4-DDE 14.08 14.62 408.7E6 352.2E6 0.079 0.073 7) Dieldrin 14.67 14.88 89321504 67012376 0.016 0.013 8) Endrin 15.18 15.54 123.9E6 103.2E6 0.036<Mt 0.030 9) Methoxychlor 17.11 18.08 133.6E6 92357488 0.073m 9,y. 0.068

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC1.D 011203P.M Wed Dec 12 11:19:07 2001 Page 1

NYC-WTC_000092401

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NYC-WTC_000092401Source: NYC Law Department, mirrored locally

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