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Pesticide quality control verification CCV2, sample AD27116, Dec 2001

Machine-extracted title · confidence 100%

Second quality control check (CCV2) for pesticide analysis showing recovery data for propachlor, methoxychlor, chlordane, toxaphene, and PCBs.

NYC-WTC_000089980–000089986

Folder label: “508 X 11/13/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011207\3PESTC3.D\ECDlA.CH Vial: 70 Signal #2 : C:\MSDCHEM\l\DATA\508\011207\3PESTC3.D\ECD2B.CH Acq On : 10 Dec 2001 8:36 am Operator: Nefliu Sample : pest ccv3 Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 21 10:22:27 2001 Quant Results File: 011208P.RES

Quant Method : C:\MSDCHEM\1\METHODS\011208P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 17 10:38:25 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds

Target Compounds 1) Propachlor 9.16 8.58 166.1E6 96611302 0.327 0.293 2) g-BHC 9.93 10.26 5485.7E6 3859.6E6 0.717m 3) Heptachlor 11.10 11.31 1587.3E6 796.7E6 0.230m 0.209 4) Aldrin 11.81 12.06 2367.4E6 1830.8E6 0.319m (31/ 0.315 5) Heptachlor Epoxi 13.25 13.41 3808.9E6 2894.7E6 0.595mj2/Y/ 0.584m 6) 4,4-DDE 14.08 14.62 5983.1E6 4871.4E6 1^019mfxqy; 1.02 0 7) Dieldrin 14.67 14.88 1362.2E6 993.1E6 .192m 8) Endrin 15.17 15.54 2160.9E6 1526.7E6 0.542m tilt,/ 0.503m 9) Methoxychlor 17.11 18.08 1795.9E6 1066.3E6 0.939m tif-/. 0.950

(f)=RT Delta >1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 3PESTC3.D 011220P.M Fri Dec 21 10:44:12 2001 , Page 1

NYC-WTC_000089981

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NYC-WTC_000089981Source: NYC Law Department, mirrored locally

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