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Toxaphene analysis results for samples TOXC1-3, Dec 2001

Machine-extracted title · confidence 90%

Chemical analysis report listing toxaphene compound concentrations and surrogate recovery metrics from December 2001.

NYC-WTC_000089559–000089567

Folder label: “508 X 11/27/01 A 12/4-12/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\011224B\TOXC1.D\ECD1A.CH Vial: 6 Signal #2 : C:\MSDCHEM\1\DATA\508\011224B\TOXC1.D\ECD2B.CH Acq On : 24 Dec 2001 3:05 pm Operator: Nefliu Sample : tox id Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 31 15:16:33 2001 Quant Results File: 011224T.RES

Quant Method : C:\MSDCHEM\1\METHODS\011224T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Wed Dec 26 10:40:08 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Cone#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.34 14.98 785.0E6 554.3E6 0.196m 0.209m Spiked Amount 0.200 Recovery 98.00% 104.50%

Target Compounds 1) Toxaphene Peak 1 14.76 15.71 29621929 14426301 0.624m 0.635m 2) Toxaphene Peak 2 15.12 16.13 53495599 64498639 0.634m 0.580m 3) Toxaphene Peak 3 15.53 16.29 31969483 23329849 0.661m 0.621m 4) Toxaphene Peak 4 17.18 16.71 115.1E6 66434362 0.606m 0.616m 5) Toxaphene Peak 5 17.55 17.79 44559225 75628707 0.583m 0.605m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. TOXCl.D 011224T.M Mon Dec 31 15:17:38 2001 Page 1

NYC-WTC_000089560

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NYC-WTC_000089560Source: NYC Law Department, mirrored locally

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