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GC/MS analysis results for sample AD23835, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23835 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089501–000089516

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089511
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT3001\23835.D Vial: 20 Acq On : 31 Oct 2001 9:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************** * Peak Number 3 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 6.57 0.46 ug/1 69289 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 'entative ID MW MolFOrm CAS# Qual 1 3-Hexanol 102 C6H14O 000623-37-0 78 2 3-Pent^ol 88 C5H12O 000584-02-1 36 3 1,2-Dutanediol 90 C4H10O2 000584-03-2 33 4 1-P/^opanamine, 2-methyl- 73 C4H11N 000078-81-9 9 Abundance Scan 166 (6.566 min): 23835.D (-) m/z 59.00 100.00% 55

asa 73 43 39 6.20 6.40 6.60 6.80 ' 7.00 49 86 ............ ' I'''' I'''' I' m/z 55.00 74.65% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63531:3-Hexanol

55

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/F 73.00 42.98% 39 4+4 I ,, .I ^4.'f'. ' I ' ' '' I ' 'I'' ' ' I ' ' ' 'I' n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62942: 3-Pentanol

31 6.20 6.40 6.60 6.80 7.00 5000 m/ z 43.00 2,7.02% 41

....... ^'87 n/z-> Abundance 20 25 30

=31-- 35 40 45 + 50 55 60 65 70 #62989:1.2-Butanediol 5b ' ' I * ' ' ' I ' '' ' I ' ' 75 80 90 " 95 AJ '-'-I = 6?20-~ 6,40 6.60\ 6.80 7.00 m/z 41.05 22.65%

5000

43 27

nZz-> 20 25 30 35 444-^4 40 I''" I'"' I"'' I" " I'''' I'"' I'''' I' 45 50 55 60 65 70 75 80 85 90 95 6.20 6.4 6.60 6.80 7.00

23835.D NP103001.M Thu Nov 01 13:23:24 2001 Page 3 / NYC-WTC_000089511

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NYC-WTC_000089511Source: NYC Law Department, mirrored locally

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