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GC/MS analysis results for sample AD23835, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23835 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089501–000089516

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089510
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT3001\23835.D Vial: 20 Acq On : 31 Oct 2001 9:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 . Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.89 ug/1 135147 1,4-Dichloroben2ene-d4 11.72 Hit# of .5 Tentative ID MW MolForm ' CAS# Qual

1 2-Hexani e 100 C6H12O'' 000591-78-6 91 2 Oxira: , 2-methyl-2-(1-methylethyl) 100 G6H12O-". 072221-03-5 72 3 2-He: inone, 4-hydroxy-3-propyl- 158 C9H18d2 062338-17-4 64 4 Me Xyl Isobutyl Ketone___________ 100 C6H12O 000108-10-1 58 'Vbundano^ Scan 151 (6.428 min): 23835.D (-) m/z 42.95 100.00% 43

58 5000

85 100 6.00 6.20 AJ 6.40 6'60 6.80 51 .1, ..................... ' I ' ' ' ' I ’ m/z 58.05 54.24% 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63387:2-Hexanone 43

58 5000 I ' ' ' ‘ I ' ' t ' ' ' ‘ I ' ' ' ' I ' ' ' 6.00 6.20 6.40 6.60 6.80 100 m/z . 57.00 18.81% 71 85

Ti^-> 20 ■ I ' ' ■ • I I I ■ ''i I

30 40 I I '' '50 ' t'p-rT-rj^TT-rT-p-rT-r-p 60 70 80 I 90 100 110 120 130 140 ■ , " • rJ Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 58 e'ciO 6.20 6.40 6.60 6.80 5000 m7z^4T705 15.60% 71 _ - ------------- _ 30-------- I I I 11 1 I I . . . , I ■ I'''' I' TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 . Abundance - #11968:2-Hexanone, 4-hydroxy-3-propyl- -------- r———........................ m/z 100.00 11.54% 58

552 29

J. 71 I 85 I I ' ’ ' ' I ’ ' ' * I 4- 100 140 . I ’ ’ • ’ I ' I ' ' 14 ' I ' ' ' ' I ' I ' ' I ' ' ' Ti/z-> -20 30 40 50 60 70 80 90 100 110 120 130 140 6:oo 6.20 6.40 6.60 6.80 .

23835.D NP103001-.M Thu Nov 01 13:23:22 2001 .. Page 2

NYC-WTC_000089510 4

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NYC-WTC_000089510Source: NYC Law Department, mirrored locally

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