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GC/MS analysis report, sample AD23721, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23721 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089234–000089246

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089242
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT1501\23721 .D Vial: 17 Acq On : 16 Oct 2001 3:49 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.76 ug/1 70738 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Te: tive ID MW MolForm CAS# Qual 1 2-Hexanoni 100 C6H12O 000591-78-6 90 2 2-Hexani :e, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 78 3 OxiraK^, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 4 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 50 Abundance Scan 158 (6.488 min): 23721 .D (-) "m/z 42795^ 100.00% 43

58 5000

- 100 ■ ■ ■ k y ,1,1, “m/z 6.20 6.40 58.05 6.60 6.80 56.80% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63384:2-Hexanone 4)3

5000 58 6.20 6.40 6.60 6.80 29 m/z 57700 17.72% J J, 71 85 100 Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone. 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 "m/z 41.05 15.88%

I'I"''''I' ---J ' I'' ‘ ' I '' ' ' I '' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' '' ' I' ' '' I ' ' ' ' r ' ' ' 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- ---- --- ------ —•—------ : - '-~6.20 - 6.40 6.60 —6.80—— ----- ““58—----- —---------------- -- m/z 100.05 12.94% 5000 71 30 85 100 I'l ' ' I ' I ' . I . .I. . I , . . . I A •• -t-[-rT-r-V‘Y-rTT--r-]--rT ' I' ' ''I' ' '' I I ■nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

23721.D NP091101.M Tue Oct 16 15:16:51 2001 Page 1

NYC-WTC_000089242

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NYC-WTC_000089242Source: NYC Law Department, mirrored locally

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