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GC/MS analysis results for sample AD23651, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.

NYC-WTC_000089059–000089072

Folder label: “GC/MS Scan 9/28/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23651.D Vial; 5 Acq On : 15 Oct 2001 4:06 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ****■*•■*■■*•**■****■**■*■■*•*****■*•■*•■*•■*•*********■*•***********■*********************.*

Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.46 Xg/1 224812 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanfone, 4-hydroxy-4-methyl- 116 C6H12O2’ 000123-42-2 53 2 Acetic cid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 3-Hydnioxy T 2 -pentanone 102 C5H10O2 003142-66-3 9 4 5-He30:;n-2-one 98 C6H10O 000109-49-9 9 Abundance / Scan 295 (7.746 min): 23651 .D (-) m/z 42795 100.00% 4b

59 5000

101 ' ' I ' ‘ ' I ' ' ' ' I ' ‘ ‘ ' I ' 7.40 7.60 7.80 8.00 .................................. 3^,1) 69 .... 83 .....I , , , , , , m/z 59.05 52.73% ■nfe-> 10 20 30 40 50 60 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000- 59 7.40 7.60 7.80 8.00 m/z 100.95 20.68% 27 101 .......................... I I ' I ' ‘ ' 1“''' ' ' I ' I J' ■ ' ' I tVz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester ---- 413------------------- _______ 7.40 7.60 7.80 8.00 5000 57 niTz 58.05 16.94% 101 15 27 I

n/z-> 10 20 30 40 50 60 70-—80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone_ _ 59' ■ ■ 3h .7.40^7..e0.^7.80 --8.00-- -m/z=4-l=?05 ■7-5-7%

5000 45 15 , , I...... I ....... I ' ' ' ‘ I ' ' ' ' I ‘ ' I l| . , .y............. ' ■ ■ I 10 20 30 40 50 60 70 80 90: 100 110 7.40 7.60 7.80 8.00

23651.D NP091101.M Wed Oct 17 10:05:16 2001 Page 2

NYC-WTC_000089067

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NYC-WTC_000089067Source: NYC Law Department, mirrored locally

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