GC/MS analysis report, sample AD23655, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23655.D Vial: 8 Acq On : 15 Oct 2001 7:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 . MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.71 ug/1 170164 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qua! . 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 ■ / 2 Acetic/acid, 1,l-dimethylethyl este 116 C6H12O2 000540-88-5 33. 3 CH2 = 'CH2C(O)OCH3 100 C5H8O2 003724-55-8 10 4 5-He: n-2-one 98 C6H10O 000109-49-9 9' • Abundance Scan 296 (7.755 min); 23655.D (-) m/z 42.95 100.00% 4)3

59 5000

101 740 7.60 7.80 8.00 .--.“-.-iL n ' ' • ' I 63 . I , H ' ' ■ ' I mTz 59705 55.90% TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000- ' • I ' • ' ■ I I ' f • I r. 59 7 40 7.60 7.80 8.00 m/z 101.05 21.23% 15 31 101 ■ ................................................. 83 I . ................... ' ' I ' I ' ' ‘ ' I ' ' ' ' I '' ' ' I ' ' ' I I ‘ ' I Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance Acetic acid, 1,1-dimethylethyl ester _ #3292:.v.

* ' I ‘ I ' ' ' ‘ I I .7 I I I >> I I I 740 7.60 7.80 8.00 5000 57 ■m/z 58.05 16.24% 101 ___________ —15 . ^„27 ' I ' '’I I I ' ' ' ' I ' ______ 10 20 30 40 50 60 70 80 90 100 110 Nsundance -#1448: CH2=CHCH2C(O)OGH3 —----------- — :8.00’ m/z 41.05 7.34% 5000-

.................................... 100 —|—I—T—r—I—T-T-T—r—r—T—I—J—|—r .......... -i--—r 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

23655.D NP091101.M Tue Oct 16 15:06:09 2001 Page 3;

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