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GC/MS analysis report, sample AD23654, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23654 showing detection of unknown compounds on October 16, 2001.

NYC-WTC_000089087–000089101

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089099
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1501\23654.D Vial: 7 Acq On : 15 Oct 2001 6:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 2.13 ug/1 208328 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 ihtative ID MW MolForm CAS# Qual

1 2-Pentano^, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50-=-* 2 Acetic aoTd, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 CH2=CH™2C (0) OCH3 100 C5H8O2 003724-55-8 10 4 Morpholine, 4-methyl-____________ 101 C5H11NO 000109-02-4 9 Abundance Scan 295 (7.751 min): 23654.D (-) m/z 4^795 100.00% 43

5000

TiZz-> Abundance 10 20 30 40 50 51 60 59

70 80 #64275: 2-Pentanone, 4-hydroxy-4-methyl- 83 I—l—I—1—1—1—f— 90 101

100 110 _L_ m/z 740 7.60 59.05 7.80 8.00 T

51.92%

4|3

5000 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 59 740 7.60 7.80 8.00 m/z 101.05 19777% 1,5 31 I, , I I , I I I , , , co , , , , , , 1 101 ,1, , , , , I I, ........... n/z-> 10 20. 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1<limethylethyl ester —4(3-.,--------- - -------------r-----------

' I ‘ ' I ' ' ' ' I ' ‘ ' I ' 7.40 7.60 7.80 8.00 5000 57 m/^ 58.05 15.64% 101 15 27 ' I ' ' ' ' I ' ' ' ’ I ‘ ' I ' ' ' ' I ' * ' ' I ' ' ' ' i. , TiZz-> 10 20' “'30 40 50 60 70 80 90 100 110 Abundance —- - --------- #1448: CH2=CHCH2C(O)OCH3 ^7X0 7.60 ~ 7.80 ~~8.00— m/^ - 41.05 7.84%

5000

58 .................................... 3^, 11 I. I I I . . I I 1 1 I . I I I . . I . I I I I I

■nZz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

23654.D NP091101.M Tue Oct 16 15:05:06 2001 Page 5

NYC-WTC_000089099

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NYC-WTC_000089099Source: NYC Law Department, mirrored locally

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