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GC/MS analysis results for sample AD23651, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.

NYC-WTC_000089059–000089072

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089066
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1501\23651.D Vial: 5 Acq On : 15 Oct 2001 4:06 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.55 ug/1 84941 1,4-Dichlorobenzene-d4 11.76 Hit# of Tentative ID MW MolForm CAS# Qual

1 2-Hexan,dne 100 C6H12O 000591-78-6 91 2 Methyl/Isobutyl Ketone 100 C6H12O 000108-10-1 58 3 2-Hexdnone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 40 4 2-Hexanone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 38 Abundance ' Scan 157 (6.479 min): 23651 .D (-) m/z 42795 100/700% .. 43

58 5000

71 85 . 100 6.20 6.40 6.60 6.80

Ti/z-> 20 30 40 41X 50 60 I I. ' I ' ‘ ' I ' ' ' ' I ' 70 80 90 100 110 120 130 140 m/z 58.05 57.85% Abundance #1556:2-Hexanone 43

58 5000 " I " ' 0 6.20 6.40 660 6.80 m/z^T?^ 16.28% 27 85 100 I k 71 I 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63350: Methyl Isobutyl Ketone

t 6.20 ............. 6.40 6.60 6.80 5000 “m/z 41.00 15.58% 58

85 100 27 I 67, I TiZz-> 20 30 40 50 60--70 - 80 90 100 110 120 130 140 Abundance , #11968: 2-Hexanone, 4-hydroxy-3-propyl- -43. '-:-6.20-----6.40-.:^-6.60:---6.80---- - -m/z^8-4-95 ■9t76% 58 Oga 29

■n/z-> ' I ' ' ' ' I ' ' ' ' I I 20 30 40 ,1, 71 85 100 , J... ?... I . ■ • ■ I...... . . .k? ' I ' ' ' ' I ' 50 60 70 80 90 100 110 120 130 140 6.20 6.40 _______ 6.60 6.80

23651.D NP091101.M Wed Oct 17 10:05:13. 2001 Page 1

NYC-WTC_000089066

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NYC-WTC_000089066Source: NYC Law Department, mirrored locally

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