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GC/MS analysis results for sample AD23652, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23652 conducted on October 16, 2001.

NYC-WTC_000089045–000089058

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089055
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1501\23652.D Vial; 4 Acq On : 15 Oct 2001 2:27 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1,00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library ; C;\DATABASE\NBS75K.L Peak Number 3 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.46 ug/1 44528 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexanoy 102 C6H14O 000626-93-7 83 2 2-Penta?fol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-Hex^ol, (R) - 102 C6H14O 026549-24-6 43 4 2-Peiyanol, 3-methyl-______________ 102 C6H14O 000565-60-6 40 Abundance Scan 185 (6.737 min): 23652.D (-) m/z 44.95 100.00% 4^

5000

r-n-q-n-TT-T-yn-TT-Tq-rn-n-Tq^ 41 56 84 87 6.40 6.60 6.80 7.00 4tU ........... I m/z 41.05 16.00% Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 415

5000 6.40 6.60 6.80 7.00 69 m/z eFToo 13.55% 19 2/31 4^1 56 I 8487 I I " I I I I ' I I I I'l I I I I I I 11 I I I I I I 1 I I I I I I "11 I 11 I I I n-rtH I I I ri i 11 i i i I | i 11 i | 11 i i | i 11 l.rl rl i,i, । i i i i । i ■n/z-> 10 15 20 ’ 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545: 2-Pentanol, 4-melhyl- --- 40-- - ;- --- --

6.40 6.60 6.80 7.00 5000 m/F" 43.05 10.12%

69 _ 39_4: , ______ 57________ |_________ 8487 ............. 27

TiZz-> Abundance 10 15 nW TI I'-'-H ' I '''' I pH I I I ‘ > I lI I I ' I H I I I I I I I 1 I I I I I I I I . I I I I I 11 I I I I I I I I I I ■ I I I 1 1 I I

20 25' 30 35 40 45 50 55 ~60 65 70 75 80 85 90 95 ___ ____ #1794: 2-Hexanol, (R)- 4□ □0 S--6.40—6.60‘■^6:80 nsZOO^^^s^ -m/ z—4-4T0 0------ rOTm

5000-

69 55 .... I..... :e4y ' I " • • I " " I ' < u j • ' • ' I > I >J I I I I I I I I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I Tlfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 >6,40 6,60 6.80 7,00^^

23652.D NP091101.M Tue Oct 16 15;02;36.2001 Page 3

NYC-WTC_000089055

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NYC-WTC_000089055Source: NYC Law Department, mirrored locally

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