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GC/MS analysis results for sample AD23650, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000089012
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search CompoundReport

Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,2-Nonadecanediol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

29.51 1.16/ug/l 141555 Chrysene-dl2 33.13

Hit# of 5 Tentative ID MW MolForm. CAS# Qua!

1 1,2-Nonadecanediol 300 C19H40O2! 039516-65-9 38 2 Penta^cane, 8-methylene- 224 C16H32. 055668-09-2 32 3 1-He^ne, 2-methyl- 98 C7H14 006094-02-6 27 4 1-Pentene, 2,4-dimethyl- 98 C7H14 002213-32-3 27 <\bundance/_ Scan 2665 (29.510 min): 23650.D (-) m/z 56700 100.00% 5

5000 41 129 iza 239 257 f 'I I T-j I' I 29.20 29.40 29.60 29.80 312 f Ti 'j T I I 1 I I I I T I' i' I 1 I j . I i' I I I I 1 I I I I I 'i I I I I I I'l 1 I ] I I I r I . ■ I' " ■ I • ■ I ■ I m/z 57.00 45747% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42822:1,2-Nonadecanediol 50 83

5000 110 269 ■p^ 124 ■ 29.20 29.40 29.60 29.80 138 m7z 47777 39736%

Tl/Z-> 20 34 40 60 1 80 100 120 140 160 180 200 220 240 260 280 300 Abundance —---------------- #28775:’Pentadecane,8-methylene^'' 53 JUU,. 29.20 29.40 29.60 29.80 5000- m/z 41.05 38.54%

/o 84 I 27 I T-| I ‘|-n |-| 196 224 r ''' I *' ‘' I' ’' ■n/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 55 ---.-- -#63261 :-1-Hexene, 2-methyl------ ,, JaA A- ; ' ' I ' “J ' I ' ' ' ' I ' ' ' n ' ' ” I • - 29.20- 29.40 -29.60 - 29.80 - m7z 55.00 29770% 41 ___ 5000- 27

I ' ' ' ‘ I Tl/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 . . - 29.20 29.40 29.60 29.80

23650.D NP091101.M Thu Oct 18 10:40:15 2001 Page 6 NYC-WTC_000089012

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NYC-WTC_000089012Source: NYC Law Department, mirrored locally

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