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GC/MS analysis results for sample AD23500, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23500 conducted on October 19, 2001.

NYC-WTC_000088826–000088852

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8 Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.383 142 146 152 rBV 24374 46099 1.75% 0.284% 2 6.484 153 157 167 rW 3 9195 100222 3.80% 0.617% 3 6.621 168 172 18 0 rW 19540 46827 1.78% 0.288% 4 6.731 180 184 193 rVB 27214 59459 2.26% 0.366% 5 11.625 713 717 727 rBV 22181 48602 1.85% 0.299%

6 11.762 727 732 754 rVB 786391 1895986 71.97% 11.678% 7 15.370 1119 1125 1143 rBV 1121966 2569646 97.55% 15.827% 8 20.658 1694 1701 1715 rBV 1221912 2634235 100.00% 16.225% 9 25.083 2176 2183 2196 rBV 1151474 2403631 91.25% 14.805% 10 29.508 2660 2665 2673 rBV 212509 392756 14.91% 2.419% 11 29.627 2673 2678 2684 rW 51212 102738 3.90% 0.633% 12 29.756 2686 2692 2700 rBV 28316 58371 2.22% 0.360% 13 30.701 2789 2795 2803 rBV 82918 161321 6.12% 0.994% 14 31.647 2892 2898 2903 rBV 155274 314084 11.92% 1.935% 15 31.739 2903 2908 2918 rW 156120 323986 12.30% 1.996% 16 32.730 3009 3016 3024 rBV 154786 313728 11.91% 1.932% 17 33T1T'6 3 05 r 3'0 5'8~ 3’0'7 0" rBV2 8“4550’5 2016195 76.54% 12.41’8% 18 33.685 3113 3120 3133 rBV 161881 368976 14.01% 2.273% 19 34.612 3215 3221 3232 rBV 116197 262415 9.96% 1.616% 20 35.503 •3312 3318 3330 rBV 92121 225487 8.56% 1.389% 21 36.366 3407 3412 3425 rBV 45981 128517 4.88% 0.792% 22 37.228 3498 3506 3512 rBV2 605692 1661395 63.07% 10.233% 23 38.376 3625 3631 3636 rBV5 7749 28890 1.10% 0.178% 24 39.716 3773 3777 3788 rVB5 6985 30469 1.16% 0.188% 25T\44'.178.„4253. 4263„42.66 rBV5 8 955 - ; .41542’ 1.58%::_ ;0.’256%

Sum of corrected areas: 16235577 23500.D NP091101.M Thu Oct 18 10:17:35 2001

NYC-WTC_000088831

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NYC-WTC_000088831Source: NYC Law Department, mirrored locally

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