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GC/MS analysis results for sample AD23319, Oct 15 2001

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Laboratory report documenting GC/MS analysis of environmental sample AD23319 conducted on October 15, 2001.

NYC-WTC_000088429–000088455

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

r LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1201\23319.D Vial: 21 Acq On : 12 Oct 2001. 9:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise ; Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location; TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.375 142 145 152 rBV 23135 45493 .1.69% 0.259% 2 6.485 153 157 168 rVV2 34842 94441 3.51% 0.538% 3 6.613 168 171 18 0 rW 20360 46345 1.72% 0.264% 4 6.733 180 184 197 rVB 25305 58847 2.19% 0.335% 5 11.626 712 717 726 rBV 21767 48202 1.79% 0.275% 6 11.763 726 732 745 rBV 793915 1915638 71.26% 10.920% 7 15.371 1119 1125 1144 rBV 1182275 2643367 98.33% 15.068% 8 20.659 1694 1701 1713 rBV 1258265 2688261 100.00% 15.324% 9 25.084 2176 2183 2194 rBV 1156263 2457565 91.42% 14.009% 10 27.324 2419 2427 2432 rBV 14113 28090 1.04% 0.160% 11 29.509 2659 2665 2672 rBV 344052 672928 25.03% 3.836% 12 29.619 2672 2677 2683 rW 69338 136542 5.08% 0.778% 13 29.748 2686 2691 2700 rW 43428 89225 3.32% 0.509% 14 30.702 2789 2795 2802 rBV 103296 204794 7.62% 1.167% 15 31.639 2892 2897 2903 rBV 238446 499685 18.59% 2.848% 16 31.731 2903 2907 2917 rW 186811 394105 14.66% 2.247% 17 31.868 2917 2922 2930 rVB2 17279 38360 1.43%' 0.219% 18 32.731 3010 3016 3023 rBV 190401 387482 14.41% 2.209% 19 33.117 3051 3058 3073 rBV2 912276 2091868 77.81% 11.924% 20 33.686 3109 3120 3132 rBV 206850 454923 16.92% 2.593% 21 34.604 3212 3220 3230 rBV 140559 329999 12.28% 1.881% 22 35.495 3312 3317 3328 rBV 113437 267430 9.95% 1.524%. 23 36.357 3406 3411 3421 rBV 57410 153678 5.72% 0.876% 24 37.230 3497 3506 3511 rBV2 636083 1750330 65.11% 9.977% 25 38.368 3624 3630 3642 rBV4 11561 45323 1.69% 0.258%

Sum of corrected areas: 17542921 23319.D NP091101.M Mon Oct 15 09:49:14 2001

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