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GC/MS analysis results for sample AD23498, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.

NYC-WTC_000088774–000088798

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088784
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT1601\23498.D Vial; 6 Acq On : 16 Oct 2001 7:07 pm ■ Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101 .M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************************************** Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.54 ug/1 54606 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 entative ID MW MolForm CAS# Qual 1 1,4-Dichlprobenzene-d4 150 C6C12D4 003855-82-1 40 2 Benzene-X 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 2-Meth; 4-6-nitroaniline 152 C7H8N2O2 000570-24-1 10 4 TisopjY ine 152 C5H4N4S 005334-23-6 10 Abundance Scan 717 (11.620 min): 23498.D (-) m/z 149.90 100.00% 1!1O

253 115 78

-n/z-> 20 ^bundance 30 40

40 JU 50 60 70 80 90 #9593:1,4-Dichlorobenzene-d4 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00 m/z 151.90 65.96%

1$0

p-' /' ' ' 1 " 5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 35.23% 35 87 ' ' I ' ' ' ' I ' ' ' ' I '' 'I...... ....... Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6^Jichloro- '1$0

115 11.20 11,40 11.60 11,80 12.00 5000 52 78 "inTz 78.05 21.63%

87

T)/z-> 20 . - . 35I 30 40 50 |- ' I ' ' ‘ ' I ' ' ' ' I ' ' ' I ' 60 70 80 90 A 100 110 120 130 140 150 160 I ' ' ' ' I

Abundance #66883: 2-Methyl-6-nrtroaniline yy---- _____--- - - -1!i2 11.20 11.40 H.60~'!1.80~~12.00~ “mTz 52.00 15.02%

553 106 52 94 l„J,..... II, 60 70 80 * I ' ' ' ' I ' ' ‘ ‘ I ' * ' I ' Ti/z-> 20 30 40 50 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23498.D NP091101.M Thu Oct 18 10:10:35 2001 Page 4

NYC-WTC_000088784

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NYC-WTC_000088784Source: NYC Law Department, mirrored locally

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