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GC/MS analysis results for sample AD23498, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.

NYC-WTC_000088774–000088798

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088783
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NYC 9/11 Public Portal Document

Library Search Compound Report Data Fiie : C:\HPCHEM\1\DATA\OCT1601\23498.D Vial: 6 Acq On : 16 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.50 ug/1 50047 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H14O 000626-93-7 83 2 2-Pentanol 4-methyl- 102 C6H14O. 000108-11-2 78 3 2-Butano 74 C4H10O 000078-92-2 50 4 Butane 2-ethoxy­ 102 C6H14O 002679-87-0 50 ^bundance Scan 185 (6.736 min): 23498. D (-) m/z 45.05 100.00% 4)5

253 41 69 6.40

Ti/z-> 10 15 20 25 4u 8659 J 73 84 87 I' ■' I" " 1111 ’ 11 ’ I' I' I • 11 ■ ■ I > I • 11 ■ I' • ■ 11' 11' I 30 35 40 45 50 55 60 65 70 75 80 85 90 95 r m/z 6.60 69.00 A 6.80 7.00 16.99% Abundance #63584: 2-Hexanol 4)5

5000 ' 6.40 6.60 ' 6.80 ' 7.00 69 m/z 41.05 16.08% ........... 19....... ........................4^1 56 1 8487. .. .................. " 111' 11" " 111111 •' • 11' 111111111' Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- ------- --------------------------- - --- - r- ---- -

6.40 6.60 6.80 7.00 5000 m/z 43.00 12.89%

27 69 42 57 I 8487 .... . ............... Il ■ 11 ■ I' • I Ti/Z^> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #334: 2-Butanol ‘ I ' ' ' ' I 4^ - -^6.40—6.60—6:80 7.00 ' ■ m/z 44.05 12.07% 5000

27 31 59 19 55 73 I'''' I' ......... . " I'"' I ‘' I" " I" " I" " I" " I' n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

23498.D NP091101.M Thu Oct 18 10:10:33 2001 Page 3

NYC-WTC_OOO688783

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NYC-WTC_000088783Source: NYC Law Department, mirrored locally

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