Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document i QuantitationReport (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm 4 7 Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 17 11:56 2001 QO Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.76 152 364186 20.00 ug/1 -0.15 19) Naphthalene-d8 15.38 136 1425437 20.00 ug/l -0.15 31) Acenaphthene-dlO 20.65 164 675442 20.00 ug/1 -0.16 49) Phenanthrene-dlO 25.08 188 962217 20.00 ug/1 -0.16 59) Chrysene-dl2 33.12 240 . 691464 20.00 ug/1 -0.16 68) Perylene-dl2 37.23 264 521377 20.00 ug/1 -0.19 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.76 132 181 0.01 ug/1 0.35 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.28 152 3675 0.21 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-FluorobiphenYl 18.80 172 1352 0.03 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = JO-OPI Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol- o.-oo 128 - 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2 -Di chlorObehz ene “' ~ '.O'.O O 146 1-0 ~ -"14) 2-Methylphenol’' 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 . __ 0 N^D. 17) N-Nitro’so-di-n-propylamine 0.00 ■’o 70 N.D. 18) Hexachloroethane 0.00 117. 0 N.D. 21) Nitrobenzene O'. 00 77 . 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP091101.M Wed Oct 17.12:09:18 2001 Page 1
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087132
Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088905
Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089418
Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069154
Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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