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GC/MS calibration report for TCLP method, Oct 2001

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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.

NYC-WTC_000088700–000088724

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C;\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GTkLOS Sample : lab blk 9/27 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 17 11:56 2001 Quant Results File: NPO91161.RES

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 - N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 0.00 128 0 ■ N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 0.00 165 0 N.D. 45) Diethylphthalate 22.16 149 2891 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0. N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. ~ 51“)—N-Ni t r os odipheny lamine OTOO" res' ' 0 ■ ■“NTD"; 52) 4-Bromophenyl-phenylether 0.00 248 0 , N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 55) Phenanthrene 0.00 178 0 N.D. 56) Anthracene 25.08 178 101 N.D. 57) Di-n-butylphthalate 27.08 149 2529“ - -N.D; - 58) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) ‘Benzidine * T- 29.28 184 1121 ntdt^ ""63) Pyrene 0.00 ~ 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 33.12 228 1532 . N.D. 6 6 )~Bi^( 2"-^thy Ihexyl) phthalate 3'3". 3 9 149 10616 N.D." 67) Chrysene 33.12 228 1532 N.D. 69) Di-n-Octylphthalate 0.00 149 0 N.D. 70) Benzo(b)fluoranthene 0.00 252 0 .. N.D. (#) = qualifier out of range (m) = manual integration LB.D NP091101.M Wed Oct 17 12:09:23 2001 Page 2 .

NYC-WTC_000088701

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