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GC/MS analysis results for sample AD23272, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.

NYC-WTC_000088456–000088484

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23272.D vial: 22 Acq On : 12 Oct 2001 10:39 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 15 Octadecane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 35.50 4.43 ug/1 421490 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Tetracosane 338 C24H50 . 000646-31-1 .91 Abundance Scan 3318 (35.498 min): 23272.D (-) m/z SYTOO 100.00% 57 43 71

85

1 I J J I 155169183197211225239253267281295 323 35.20 35.40 35.60 35.80 m/z 71705 73741% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance ’ #71561: Octadecane 5|7 43 71 85 I 5000 T 35.20 35.40 35.60 35.80 99 m/z 43.05 68.83% A n/z-> 40 60 X ''''I''''I''''I''''I''''I' ' ‘'I '''' I'' ' ‘ I' ''' I ''' ‘ I'' ' ‘ I ‘ ‘' I ‘' 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance 43 57

71 #39862; Eicosane

,... R.... 35.20 35.40 35.60 35.80 5000- 85 m/z 85.05 49.37%

I, 7113127141155 196 240 282 I' ''' I nrp-rrrY “^1'''' i Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201; Heneicosane 35.20 35.40 35.60 35.80 71 m/z 54.95 25.28%

5000 85 I 99 268 296 I ‘ ' I ' ' ' ' I ■p-n-rp-r-r-t-p •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.20 35.40 35.60 35.80

23272.D NP091101.M Mon Oct 15 09:42:21 2001 Page 15

NYC-WfC_00b08'8477

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NYC-WTC_000088477Source: NYC Law Department, mirrored locally

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