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GC/MS analysis results for sample AD23272, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.

NYC-WTC_000088456–000088484

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088476
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report “ t

Data File : C:\HPCHEM\1\DATA\OCT1201\23272.D Vial: 22 Acq On : 12 Oct 2001 10:39 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.61 4.73 ug/1 506473 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm' CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91 2 Heptacosane 380 C27H56 000593-49-7 91 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Pentacosane 352 C25H52 000629-99-2 91 Abundance Scan 3221 (34.607 min): 23272.D (-) m/z SYTOO 100.00% 57

5000 85

4

■n/z-> Abundance JLuL J, .ll T j '’f. , 1^^ . 197 225 267_________________ frrrlYrrlHyl'VrrfTTTVp-^TTT+TTTYTTTTyrTTTpTm-iTTTTyrTTTpTTT^^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #42201: Heneicosane 34.20 34.40 34.60 34.80 35.00 ■m/z 71710 72.03%

57

5000 85 2 34.20 34.40 34.60 34.80 35.00 ■m/z 43705 68.18% I 113 T J tJJSXh I' 1111 »' " I " ' 11' 1111' " ' I I" " I" " I 268 296 p-rrrp-rrtT-r I ' • " I • ’' * I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248: Heptacosane 57

34.20 34.40 34.60 34.80 35.00 5000 85 m/z 85.05 48.73% A

If"* , 169 196 224 281 324 380

n " I' " ' I ‘ I' ‘ " I " " I'' ' I'''' I" " I'''' I'''' I"'' I'''' I'''' I'''' I''" I'' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #51002: Heneicosane, 11 -(1 .ethylpropyl)- 43 34.20 34.40 34.60 34.80.35.00 m/z 41.05 24.86% 71 5000

, 183 225 295 338 I'' ‘' I'''' I''' j ''‘' I' " ' I ‘" I I'''' I'' " I' ’ ‘' I'''' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 34.20 34.40 34.60 34.80 35.00

23272.D NP091101.M Mon Oct 15 09:42:19 2001 Page 14

NYC-WTC_000088476

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