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GC/MS analysis results for sample AD23084, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23084 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087904–000087919

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\OCT0401\23084.D Vial: 4 Acq On 4 Oct 2001 6:27 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : G:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.379 141 146 153 rBV 19995 48125 1.20% 0.225% 2 6.489 154 158 169 rW 31299 89822 2.24% 0.421% 3 6.737 181 185 192 rW 20834 45110 1.13% 0.211% 4 11.639 715 719 729 rVB 29685 73630 1.84% 0.345% 5 11.786 729 735 748 rBV 1077548 2784095 69.57% 13.036%

6 15.394 1122 1128 1145 rBV 1788421 3833693 95.80% 17.951% 7 20.682 1697 1704 1723 rBV 1856438 4001696 100.00% 18.737% 8 25.107 2179 2186 2197 rBV2 1643469 3729248 93.19% 17.462% 9 27.108 2399 2404 2411 rBV 52657 107357 2.68% 0.503% 10 29.532 2662 2668 2676 rBV 42424 81020 2.02% 0.379%

11 30.725 2793 2798 2803 rBV2 27913 57446 1.44% 0.269% 12 31.671 2896 2901 2906 rBV 31541 61485 1.54% 0.288% 13 31.763 2906 2911 2921 rVB 32767 65683 1.64% 0.308% 14 32.754 3014 3019 3026 rBV 34846 67068 1.68% 0.314% 15 33.158 3055 3063 3076 rBV2 1316346 3226995 80.64% 15.110%

16 33.709 3116 3123 3129 rBV2 40602 88908 2.22% 0.416% 17 34.636 3220 3224 3231 rVB2 31717 66129 1.65% 0.310% 18 35.527 3316 3321 3330 rBV 24364 53256 1.33% 0.249% 19 36.390 3409 3415 3423 rBV2 16891 41014 1.02% 0.192% 20 37.271 3501 3511 3533 rBV2 976282 2835106 70,85% 13.275%

Sum of corrected areas: 21356886

23084.D NP091101.M Tue Oct 09 12:28:38 2001

NYC-WTC_000087909

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NYC-WTC_000087909Source: NYC Law Department, mirrored locally

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