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GC/MS analysis results for sample AD22976, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22976 conducted on October 15, 2001, identifying unknown compounds.

NYC-WTC_000087863–000087874

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document j-iinrary bearen compound Report

Data File : C:\HPCHEM\1\DATA\OCT1101\22976.D vial: 7 Acq On : 11 Oct 2001 3:37 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASfi\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.48 ug/1 63238 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-HexanoV 102 C6H140 000626-93-7 78 2 2-Penta;E(ol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Hex^ol, (R) - 102 C6H14O 026549-24-6 56 4 2-HeXanol, (S) -________________________ 102 C6H14O 052019-78-0 56 Abundance / Scan 184 (6.730 min): 22976.D (-) m/z 44795 100.00% 4)5

552

41 69 84 87 6.40 6.60 6.80 7.00

Tl/z-> ^.44 ................. Il ym 11' I " I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z 69700 7777271 Abundance #63584: 2-Hexanol 4)5

A A A 5000 6.40 6.60 6.80 7.00 69 m/z 41705 13.78% 8487 Tife-> 10 15 19 20 25 30 35 56 pv:-(P- 4 40 45 50 55 60 65 70 75 80 85 90 95 <\bundance #63545: 2-Pentanol, 4-methyl- 4)5

6.40 6.60 6.80 7.00 5000 m/z 44.05 9.42%

69 2,^ 3942 , 57 I 84^ I'''' I'''' I'''' I' I'' I I' 111" I" " I"' N ” " I ” " I''' h' I" I" " I" -l-r TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ^bundance #1794: 2-Hexanol, (R)- 4fe 6.40 6.60 6.80 7.00 m/z 427717 8797%

552

1^ 3942, 69 19 55 8487 10 15 20 -rr p T ‘' I''' 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 A 6.40 6.60 6.80 7.00

22976.D NP091101.M Mon Oct 15 08:40:53 2001 Page 2

NYC-WTC_000087872

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NYC-WTC_000087872Source: NYC Law Department, mirrored locally

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